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MCCampbellAnalVtical, Inc. 1534 Willow Pass Road,Pittsburg,CA 94565-1701 <br /> Web:www.mccampbell.com E-mail:main@mccampbell.com <br /> "When Ouelity Counts" I Telephone,877-252-9262 Fax:925-252-9269 <br /> • QC SUMMARY REPORT FOR SW8015C <br /> W.O.Sample Matrix: Water QC Matrix: Water WorkOrder: 0805464 <br /> EPA Method SW8015C Extraction SW3510C BatchlD:35612 Spiked Sample ID: NIA <br /> Analyte Sample Spiked MS MSD MS-MSD LCS _CSD LCS-LCSD Acceptance Criteria(%) <br /> pg/L pg/L %Rec. %Rec. %RPD % Rec. %Rec. %RPD MS/MSD RPD LCS/LCSD I RPD <br /> TPH-Diesel(C 10-C23) N/A 1000 N/A N/A N/A 121 121 0 N/A I N/A 70- 130 30 <br /> %SS: N/A 2500 N/A N/A N/A 117 117 0 N/A 1 N/A 70- 130 30 <br /> All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions: <br /> NONE <br /> BATCH 35612 SUMMARY <br /> Lab ID Date Sampled Date Extracted Dale Analyzed Lab ID Date Sampled Date Extracted Date Analyzed <br /> 0805464-011A 05/16/08 10:45 AM 05/16/08 05/21/08 8:13 AM 0805464-012A 05/16/08 11:15 AM 05/16/08 05/17/08 5:31 PM <br /> 0805464-013A 05/16/08 11:30 AM 05/16/08 05/21/08 1:22 AM 0805464-OI4A 05/16/08 11:45 AM 05/16/08 05/17/08 7:44 PM <br /> • <br /> MS=Matrix Spike;MSD=Matrix Spike Duplicate;LCS=Laboratory Control Sample;LCSD=Laboratory Control Sample Duplicate;RPD=Relative Percent Deviation. <br /> %Recovery=100'(MSSample)/(Amount Spiked);RPD=100`(MS- MSD)/((MS+MSD)/2). <br /> MS/MSD spike recoveries and/or%RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons:a)the sample is inhomogenous AND <br /> contains significant concentrations of analyte relative to the amount spiked,or b)the spiked sample's matrix interferes whh the spike recovery. <br /> N/A=not enough sample to perform matrix spike and matrix spike duplicate. <br /> NR=analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content. <br /> 42 <br /> DHS ELAP Certification No 1644 QA/QC Officer <br /> • <br />