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1534 Willow <br /> McCamubell Analytical, Inc. :wwwmcca.pbslLconn Pittsburg,CA 94565-1701 <br /> Web:www.mccamp6ell.wm E-mail:mein@mccampbell.com <br /> "When Oualitv Counts" I Telephone-977-252-9262 Fax:925-252-9269 <br /> • QC SUMMARY REPORT FOR SW8015C <br /> W.O.Sample Matrix: Soil QC Matrix: Soil WorkOrder: 0805464 <br /> EPA Method SW8015C Extraction SW3550C BatchlD: 35677 Spiked Sample ID: 0805420.013A <br /> Sample Spiked I MS I MSD MS-MSD LCS LCSD LCS-LCSD Acceptance Criteria(%) <br /> Analyte <br /> mg/Kg mg/Kg %Rec. e/Rec.I %RPD I%Rec. %Rec. %RPD MS/MSD RPD LCS/LCSD RPD <br /> TPH-Diesel(C 10-C23) ND 20 126 124 1.55 116 113 2.22 70- 130 30 70- 130 30 <br /> a%SS; 118 50 119 117 1.98 94 96 1.65 70- 130 30 70- 130 30 <br /> All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions: <br /> NONE <br /> BATCH 35677 SUMMARY <br /> Lab ID Date Sampled Date Extracted Date Analyzed Lab ID Date Sampled Date Extracted Dale Analyzed <br /> 0805464-001A 05/16/08 8:05 AM 05/16/08 05/18/08 9:29 PM 0805464-002A 05/16/08 7:55 AM 05/16/08 05/17/08 6:38 PM <br /> 0805464-003A 05/16/08 8:15 AM 05/16/08 05/23/08 9:00 AM 0805464-004A 05/16/08 8:35 AM 05/16/08 05/17/08 7:44 PM <br /> 0805464-005A 05/16/08 8:35 AM 05/16/08 05/17/08 11:03 PM 0805464-006A 05/16/08 9:00 AM 05/16/08 05/18/08 2:22 AM <br /> 0805464-007A 05/16/08 9:15 AM 05/16/08 05/23/08 9:02 AM <br /> • <br /> MS=Matrix Spike;MSD=Matrix Spike Duplicate;LCS=Laboratory Control Sample; _CSD=Laboratory Control Sample Duplicate;RPD=Relative Percent Deviation. <br /> %Recovery=too'(MS-Sample)/(Amount Spiked);RPD=100-(MS- MSD)/((MS+MSD)12). <br /> MS/MSD spike recoveries and/or%RPD may fall outside of laboratory acceptance crilena due to one or more of the following reasons:a)the sample is inhomogenous AND <br /> contains significant concentrations of analyte relative to the amount spiked,or b)the spiked sample's matrix interferes with the spike recovery. <br /> N/A=not enough sample to perform matrix spike and matrix spike duplicate. <br /> NR=analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content. <br /> DHS ELAP Certification N°1644 QA/QC Officer <br /> • <br />