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10 Second Avenue South,##D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br />' 24 http//www mccampbelI com E-mail main@mccampbell com <br /> Date Sampled 05/29/98 <br /> Advanced GeoEnvironmental Client Project ID Ripon Farm Service <br /> 4005 North Wilson Way Date Received 06/02/98 <br />' Client Contact Bill Little Date Extracted 06/04/98 <br /> Stockton,CA 95205 <br /> ' Client P O Date Analyzed 06/04/98 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> ' Lab ID 89906 <br /> Client 1D MW8/5-29-98 <br /> Matrix W <br /> ' Compound Concentration* Compound Concentration* <br /> Acetone' ' ND<5 Ethylbenzene ND <br /> Benzene NO Hexach]orobutadiene NO <br /> Bromobenzene NO lodomethane NO <br /> ' Bromochloromethane NO Isopropylbenzene NO <br /> Bromodichloromethane NO p-Isopropyl toluene I 1 <br /> Bromoform NO Methyl butyl ketoneNO <br /> Bromomethane NO Methylene Chloride"' ND <br /> ' n-Butyl benzene 36 Methyl ethyl ketone' NO <br /> sec-Butyl benzene I1 Methyl isobutyl ketone's NO <br /> tert-Butyl benzene NO Methyl tert-Butyl Ether(MTBE) -- <br /> Carbon Disulfide 1 9 Naphthalene ND<15 <br /> Carbon Tetrachloride NO n-Propyl benzene NO <br /> Chlorobenzene NO Styrene` ' ND <br /> Chloroethane NO 1,1,1,2-Tetrachloroethane NO <br /> 2-Chloroethyl Vinyl Ethe NO 1,1 2,2-Tetrachloroethane NO <br /> ' Chloroform 1 6 Tetrachloroethene NO <br /> Chloromethane NO Toluene" NO <br /> 2-Chloratoluene NO 1,2 3-Trichlorobenzene NO <br /> ' 4-Chlorotoluene NO 1,2 4-Trichlorobenzene NO <br /> Dibromochloromethane ND 11 1-Trichloroethane NO <br /> 12-Dibromo-3-chloropropane NO 1,1 Z Trichloroethane NO <br /> Dibromomethane NO Trichloroethene ND <br /> ' 1,2-Dichloroben7ene NO TrichlOTUfluoTomelhane ND <br /> 1,3-Dichlorobenzene NO 1,2,3 Trichloropropane NO <br /> 1,4-Dichlorobenzene NO 12,4-Trtmethylbenzene NO <br /> Dichlorodifluoromethane NO 1,3,5 Tnmethylbenzene NO <br /> 1,1-Dtchloroethane NO Vtn}I Acetate"" NO <br /> ' 1,2-Dtchloroethane 20 Vinyl Chloride"' NO <br /> 1 1-Dichloroethene NO Xylenes,total 1O1 NO <br /> cis-1,2-Dichlovoctbenc NO <br /> ' <br /> trans-1,2 Dichloroethene NO <br /> 1,2-Dichloropropane NO <br /> 1,3-Dichloropropane ND <br /> 2,2-Dichloropropane NO Comments <br /> ' 1,1-Dichloropropene NO Surrogate Reco,,eries <br /> cis-1,3-Dichloropropene NO Dibromofluoromethane 109 <br /> trans-l,3-Dichloropropene ND Toluene-d8 94 <br /> Ethylene dibromide NO 4-Bromofluorobenzene 90 <br /> ' water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug1L <br /> Reporting limits unless otherwise stated water samples i ug/L vapor samples 0 5ug/L solid and sludge samples 5 ug/kg,wipes 0 2ug/wipe <br /> . ND means not detected above the reporting limit,NIA means analyte not applicable to this analysts <br /> &Reporting limit raised due to ion interference <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy)ethene, (d) 2-hexanone (e)dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present (i)liquid sample that contains greater than —5 vol % <br /> sediment 0)sample diluted due to high organic content,(k)peaks present in this carbon range do not match the panem of our standard fo <br /> this analyte,(1)methylbenzene;(m)acetic acid ethenyl ester (n)chloroethene (o)ditnethylbenzenes <br /> ' DHS Certification No 1644 / Edward Hamilton,Lab Director <br />