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10 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> ' http//www mccampbell com E-mail main@mecampbell com <br /> t Advanced GeoEnvtronmentalp Date Sampled 05/29/98 <br /> Client Project ID Ripon Farm Service <br /> 4005 North Wilson Way Date Received 06/02/98 <br /> Stockton,CA 95205 Client Contact Bill Little Date Extracted 06/05/98 <br /> ' Client P O Date Analyzed 06/05/98 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 89907 <br /> Client ID V W 1 /5-29-98 <br /> Matrix W <br /> ' Compound Concentration* Compound Concentration* <br /> Acetone ND<500 Ethylbenzene 830 <br /> Benzene 2200 Hexachlorobutadiene ND<100 <br /> Bromobenzene ND<100 lodomethane ND<100 <br /> Bromochloromethane ND<100 Isopropylbenzene ND<100 <br /> Bromodichloromethane ND<100 p-Isopropyl toluene ND<100 <br /> Bromoform ND<100 Methyl butyl ketone' ' ND<100 <br /> Bromomethane ND<100 Methylene Chloride"' ND<100 <br /> n-Butyl benzene ND<]00 Methyl ethyl ketone ND<100 <br /> sec-Butyl benzene ND<100 Methyl isobutyl ketones ND<100 <br /> tert-Butyl benzene ND<100 Methyl tent-Butyl Ether(MTBE) --- <br /> Carbon Disulfide ND<100 Napthalene 660 <br /> Carbon Tetrachloride ND<100 n-Propyl benzene 150 <br /> Chlorobenzene ND<100 Styrene' ND<100 <br /> Chloroethane ND<100 1,1 1,2-Tetrachloroethane ND<100 <br /> ' 2-Chloroethyl Vinyl Ether` ND<100 1,1 2 2 Tetrachloroethane ND<100 <br /> Chloroform ND<100 Tetrachloroethene ND<100 <br /> Chloromethane ND<100 Toluene"' N13<100 <br /> 2-Chlorotoluene ND<100 1,2,3-Tnehlorobenzene ND<100 <br /> 4-Chlorotoluene ND<100 1 2 4 Trichlorobenzene ND<100 <br /> Dibromochioromethane ND<100 1,1 1-Trichloroethane ND<100 <br /> 12-Dibromo-3-chloropropane ND<100 112-Tricliloroethane ND<100 <br /> Dibromomethane ND<100 Tnehloroethene ND<100 <br /> 1,2-Dichlorobenzene ND<100 Trichlorofluoromethane ND<100 <br /> 1,3-Dichlorobenzene ND<100 1,2,3-Tnchloropropane ND<100 <br /> 1,4 Dichlorobenzene ND<100 1,2 4-Trimethylbenzene 560 <br /> Dichlorodifluoromethane ND<100 1,3,5-Trmiethylbenzene 150 <br /> ' <br /> 1,1-Dichloroethane ND<100 Vinyl Acetate p11 ND<100 <br /> 1,2-Dichloroethane 520 Vmyl Chloride°' ND<100 <br /> l,l-Dichloroethene ND<100 Xylenes,total '°' 920 <br /> cis-1,2-Dichloroethene ND<100 <br /> trans-1,2-Dichloroethene NiX100 <br /> 1,2-Dichloropropane ND<100 <br /> 1,3-Dichloropropane ND<100 <br /> 2,2-Dichloropropane ND<100 Comments <br /> ' 1,1-Dtchloropropene Nl <100 Surrogate Recoieries(%) <br /> cis-1,3-Dichloropropene ND<100 Dibromotluoromethane 111 <br /> trans-1,3-Dichloropropene ND<100 Toluene-d8 94 <br /> Ethylene dibromide ND<100 4-Bromofluorobenzene 87 <br /> water and vapor samples are reported to ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP I SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 0 5 ug/L vapor samples 0 5 ug/L solid and sludge samples 5 ug/kg, wipes <br /> 0 2ug/wipe ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> (b) 2-prop2none or dimethyl ketone, (c) (2-chloroethoay)ethene (d) 2-hexanone, (e)dichloromethane (i) 2-but2none (g) 4-methyl-2- <br /> ' pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (1)liquid sample that contains greater than —5 vol % <br /> sediment,0)sample diluted due to high organic content (k)peaks present in this carbon range do not match the pattern of our standard fo <br /> this analyte,(1)methylbenzene;(m)acetic acid ethenyl ester,(n)chloroethene (o)dimethylbenzenes <br /> DHS Certification No 1644 // Edward Hamilton,Lab Director <br />