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1 4 July 16, 2004 Lab ID SP 406530 ' Ground Zero Analysis Customer 3-14996 Quality Control - Organic ' Constituent Method Date/ID Type Units Conc QC Data DQO Note ' n-Burylbertzene 5242 07/07/2004 A209 BS ug/L 1000 964% 89-158 BSD ug/L 1000 942% 89-158 BSRPD ug/L 2 3% 515 3 ' 5242 07/07/2004 A GO-CCv ug/L 1000 113% 70-130 sec-Butylbenzene 5242 07/07/2004 A209 Blank ug/L ND <0 5 BS ug/L 1000 920% 92-147 SSD ug/L 1000 88 0% 92-147 435 ' 13SRPD ug/L 45% 515 3 5242 07/07/2004 A 00-CCv ug/L 1000 113% 70-130 ' tert-Burylbenzene 5242 07/07/2004 A209 Blank ug/L ND <05 BS ug/L 1000 95 3% 79-140 BSD ug/L 1000 894% 79-140 BSRPD ug/L 65% :!5 15 8 ' 5242 07/07/2004 A OD-CCv ug/L 1000 112% 70-130 Carbon Tetrachloride 5242 07/07/2004 A209 Blank ug/L ND <0 5 BS ug/L 1000 908% 80-151 BSD ug/L 1000 864%9% 80-151 4 BSRPD ug/L 4 9% 520 6 5242 07/07/2004 A 00-CCv ug/L 1000 903% 70-130 ' Chlorobenzene 5242 07/07/2004 A209 Blank ug/L ND <0 5 BS ug/L 1000 82 8% 74-134 BSD ug/L 1000 78 4% 74-134 BSRPD ug/L 5 5% 516 9 ' 5242 07/07/2004 A 00-CCv ug/L 1000 90 1% 70-130 Chloroethane 5242 07/07/2004 A209 Blank ug/L ND <05 ' BS ug/L 1000 967% 80-173 BSD ug/L 1000 90 1% 80-173 BSRPD ug/L 70% 516 1 5242 07/07/2004 A 00-CCv ug/L 1000 964% 70-130 ' Chloroform 5242 07/07/2004 A209 Blank ug/L ND <05 BS ug/L 1000 107% 78-141 BSD ug/L 1000 95 9%O 78-141 ' BSRPD ug/L 106% 517 6 5242 07/07/2004 A 00-CCv ug/L 1000 104% 70-130 Chloromethane 5242 07/07/2004 A209 Blank ug/L ND <05 ' BS ug1L 1000 935% 68-165 BSD ug/L 1000 85 8% 68-165 BSRPD ug/L 86% 515 7 5242 07/07/2004 A 00-CCv ug/L 1000 90 9% 70-130 2-Chlorotoluene 5242 07/07/2004 A209 Blank ug/L ND <0 5 Report continued on next page SP 406530 Quality Control Page 2 1