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I July 16, 2004 Lab TD SP 406530 ' Ground Zero Analysis Customer 3-14996 Quality Control - Organic ' Constituent Method Date/ID Type Units Cone QC Data DQO Note ' 2-Cb1oratoluene 5242 07/07/2004 A209 BS ug/L 1000 951% 83-155 BSD ug/L 1000 88 6% 83-155 BSRPD ug/L 70% 517 1 ' 5242 07/07/2004 A 00-CCV ug/L 1000 113% 70-130 4-Chlorotoluene 5242 07/07/2004 A209 Blank ug/L ND <05 BS ug/L 1000 904% 87-146 BSD ug/L 1000 87 0% 87-146 ' BSRPD ug/L 3 8% 515 6 5242 07/07/2004 A 00-CCV ug/L 1000 110% 70-130 ' Di-tsopropyl ether (DIPS) 5242 07/07/2004 A209 Blank ug/L ND <3 BS ug/L 1000 98 2% 76-146 BSD ug/L 1000 91 3% 76-146 BSRPD ug/L 069 53 00 ' 5242 07/07/2004 A 00-CCV ug/L 1000 88 1% 70-130 Dtbromochloromethane 5242 07/07/2004 A209 Blank ug/L ND <05 BS ug/L 1000 996% 82-143 BSD ug/L 1000 869% 82-143 BSRPD ug/L 13 5% :519 4 5242 07/07/2004 A 00-CCV ug/L 10 00 97 6% 70-130 ' Dtbromomethane 5242 07/07/2004 A209 Blank ug/L ND <05 BS ug/L 1000 100% 87-132 SSD ug/L 1000 89 1% 87-132 BSRPD ug/L 11 8% 519 3 ' 5242 07/07/2004 A 00-CCV ug/L 1000 101% 70-130 1,2 Dichlorobenzene 5242 07/07/2004 A209 Blank ug/L ND <0 5 ' BS ug/L 1000 103% 86-147 BSD ug1L 1000 945% 86-147 BSRPD ug/L 85% 1 520 6 5242 07/07/2004 A 00-CCV ug/L 1000 120% 70-130 ' 1 3-Dichlorobenzene 5242 07/07/2004 A209 Blank ug/L ND <0 5 BS ug/L 1000 976% 87-141 BSB ug/L 1000 895% 87-141 ' 13SRPD ug/L 86% 516 2 5242 07/07/2004 A 00-CCV ug/L 1000 115% 70-130 1,4-Dichlorobenzene 5242 07/07/2004 A209 Blank ug/L ND <05 ' BS ug/L 1000 965% 86-146 BSD ug/L 1000 860% 86-146 BSRPD ug/L 11 6% 518 6 5242 07/07/2004 A 00-CCV ug/L 1000 113% 70-130 1 2 Dichlorobenzene-d4 Surrogate 5242 07/07/2004 A209 Blank ug/L 1 1000 88 8% 70-130 Report continued on next page SP 406530 Quality Control Page 3