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110 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//www mccampbell com E-mail main@mccampbell corn <br /> I Advanced GeoEnvironmentalDate Sampled 07101-03/98 <br /> Client Project ID Cal-Fuels <br /> Date Received 07/09/98 <br /> 4005 North Wilson Way <br /> Stockton, CA 95205 Client Contact Tim Cuellar Date Extracted 07/10/98 <br /> Client P O Date Analyzed 07/10-07/13/98 <br /> Volatile Organics By GUMS <br /> EPA method 8264 <br /> Lab ID 91878 <br /> I Client ID MW11-25 <br /> Matrix S <br /> Compound Concentration* Compound Concentration* <br /> I Acetone` ' ND<50 Ethytbenzene ND <br /> Benzene ND Hexachlorobutadiene ND <br /> Bromobenzene ND ]odomethane ND <br />' Bromochloromethane ND Isopropylbenzene ND <br /> Bromodichloromethane ND p-Isopropyl toluene ND <br /> Bromofonn ND Methyl butyl ketone' ' ND <br /> Bromomethane ND Methylene Chlonde" ND<15 <br /> n-Butyl benzene ND Methyl ethyl ketone"I ND <br /> sec-Butyl benzene ND Methyl isobutyl ketone'x ND <br /> tert-Butyl benzene ND Methyl ten-Butyl Ether(MTBE) <br /> Carbon Disulfide ND Naphthalene ND <br /> Carbon Tetrachloride ND n-Propyl benzene ND <br /> C'hlorobenzene ND Styrene' ND <br /> Chloroethane ND 1,1 12-Tetiachloioethane ND <br /> 2-Chloroethyl Vinyl Ether"' ND 1,1 2,2-Tetrachioroethane ND <br /> Chloroform ND Teirachloroeihene ND <br /> Chloromethane ND Toluene" ND <br /> 2-Chlorotoluene ND 12,3-Trichlorobenzene ND <br /> 4-Clilorotoluene ND 1 2 4-Trichlorobenzene ND <br /> I Dibromochloromethane ND i 1 1-Trichloroethane ND <br /> 1 2-Dibromo-3-chloropropane ND 1,1,2-Trichloroethane ND <br /> Dibromomethane ND Trichloroethene ND <br /> 1 2-Dichlorobenzene ND Trichlorofluoromethane ND <br /> 1 3-Dichlorohenzene ND 1 2 3-Trichloropropane ND <br /> 14-Dichiorobenzene ND 1 2 4-Trimethylbenzene ND <br /> Dichlorodifluoromethane ND l 3 5-Tri met hylbenzene_ ND <br /> 1 i-Dichloioethane ND Vinyl Acetate""' ND <br /> 1 2-Dichioroethane ND Vinyl C hloride"" ND <br /> I 1-Dichloroethene ND Xylenes total '°' ND <br /> cis-1,2-Dichloroethene ND <br /> trans 12-Dichloroethene ND <br /> 1 1,2-Dichloropropane ND <br />. 1,.3-llichloropropane NU <br /> 2 2-Dichloropropane ND Comments <br /> 1,1-Dichloropropene ND Surrogate Reco%cries(1/4) <br /> cls-l3-Dichloropropene ND Dibrornofluoiomethane 102 <br /> trans-1,3-Dichloropropene ND Toluene-d$ 105 <br /> Ethylene dibromide ND 4-Bromotluorobenzene 110 <br /> Nater and vapor samples are reported in ug/L,soil and sludge samples, ug/kg Nipes m ugAv,pe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 0 ug/L, %apor samples 05 ug/L solid and sludge samples 5 uglkg wipes <br /> 0 2ug/wipe ND means not detected above the reporting limit,N/A means analyte not applicable to this analvsis <br /> (b) 2-propanone or dimethyl ketone (c) (2-chloroethoxy) ethene (d) 2-hexanone (e) dichloromethane, (f) 2-butanone (g) 4-methyl-2 <br />' pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than —5 vol % <br /> sediment 0)sample diluted due to high organic content,(k)peaks present in this carbon range do not match the pattern of our standard fo <br /> this analyte (1)methylbenzene,(m)acetic acid ethenyl ester (n)chlornethene (o)dimethylbenzenes <br /> DHS Certification No 1644 _Edward Hamilton, Lab Director <br /> I <br />