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110 Second Avenue South,#tD7, Pacheco,CA 94553-5560 <br /> 4 McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//www mccampbell com E-mail main@mccampbell com <br /> IAdvanced GeoEnvirotrmental Client Project ID Cal-Fuels Date Sampled 07/01-03/98 <br /> 4005 North Wilson Way Date Received 07/09/98 <br /> Stockton, CA 95205 Client Contact Tim Cuellar Date Extracted 07/10/98 <br /> Client P O Date Analyzed 07/10/98 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 91879 <br /> Client ID M W 11-40 <br /> Matrix S <br /> Compound Concentration* Compound Concentration* <br /> Acetone` ' ND<50 Ethylbenzene ND <br /> Benzene ND Hexachlorobutadiene ND <br /> Bromobenzene ND lodomethane ND <br /> Bromochloromethane ND Isopropyibenzene ND <br /> Bromodiebloromethane ND p-Isopropyl toluene ND <br /> Bromoform ND Methyl butyl ketone` ' ND <br /> Bromomethane ND Methylene Chlonde1" ND<15 <br /> n-Butyl benzene ND Methyl ethyl ketone" ND <br /> sec-Butyl benzene ND Methyl isobutyl ketone`° ND <br /> tert-Butyl benzene ND Methyl teri-Butyl Ether(MTBE) <br /> C arbon Disulfide ND Naphthalene ND<50 <br /> Caibon Tetrachloride ND n-Propvl benzene ND <br /> Chlorobenzene ND Serene" ND <br /> Chloroethane ND 1,1 1 2-Turathloroeihane ND <br /> 2-Chloroethyl Vinyl Ether"' ND 1 1 2 2-Tetiachloroethane ND <br />' Chloroform ND Tetrachloioethene ND <br /> Chloromethane ND Toluene" ND <br /> 2-Chloiotoluene ND 123-Trichlorobenzene ND <br /> 4-C hlorotoluene ND l 2 4-Trichlorubenzene ND <br />' Dibromochloromethane ND I 1 1-Trichloroethane ND <br /> I2-Dtbromo-3-chloropropane ND 1 12-Tiichloroethnne ND <br /> Dibromomethane ND Trichloroethene ND <br /> 12-Dichlorobenzene ND Trichlorofluoromethane ND <br /> 13-Dichlorobenzene ND 1 2 3-Trichloropropane ND <br /> I 4-Dichlorobenzene ND 1 2 4-Trim0hylbenzene ND <br /> Dichlorodifluoromethane ND 1 3 5-Trimethylbenzene ND <br /> I i-Dichloroethane ND Vinyl Actiate""' ND <br /> 12-Dichloroethane ND Vinvl Chloride"" ND <br /> 1 1-Dichloroethene ND A}lenes total '°' ND <br /> cis-1 2-Dichloroethene ND <br /> trans-1,2-Dichloroethene ND <br /> 1 2-Dichloropropane ND <br />. i 3-Dicnioropropane ND <br /> 2 2-Dichloropropane ND Comments <br /> 1,1-Dichloropropene ND Surrogate Reco%cries(%) <br />' Cis-1,3-Dichloropropene ND Dibromntluoromethane 103 <br /> trans-1,3-Dichloropropene ND Toluene-d8 109 <br /> Ethylene dibromide ND 4-Bromotluorobenzene 108 <br /> Hater and vapor samples are reported in ug/L soil and sludge samples m ug/kg ,,p,,,n ug/w[pe and all TCL?/SPLP extracts in uglL <br /> Reporting limits unless otherwise stated water samples 1 0 ug/1- tiapor samples 05 ug/L, solid and sludge samples 5 ug/kg, wipes <br /> 0 2ug/wipe ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone (c) (2-chloroethoxy) ethene (d) 2-hexanone (e) dichloromethane (1) 2-butanone (g) 4-methyl-2 <br /> pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present (i)liquid sample that contains greater than —5 vol % <br /> sediment (I)sample diluted due to high organic content (k)peaks present in this carbon range do not match the pattern of our standard fo <br /> this analyte (1)methylbenzene,(m)acetic acid ethenyl ester (n)chloroethane (o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />