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i <br /> 110 Second Avenue South,#D7, Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http I/www mccampbell com E-mail main@mccampbell corn <br /> Advanced GeoEnvironmentalClient Project 1D Cal Fuels Date Sampled 07116-07117198 <br /> 4005 North Wilson Way Date Received 07/22/98 <br /> Stockton, CA 95205 Client Contact Tim Cuellar Date Extracted 07/29/98 <br /> Client P O Date Analyzed 07/29-07130/98 <br /> 1 Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 92546 <br /> t Client ID MWI-7117198 <br /> iMatrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone` ' ND<100 Ethylbenzene 160 <br /> Benzene 510 Heraclilorobutadiene ND<25 <br /> Bromobcnzene ND<25 lodomethane ND<25 <br /> Bromochloromethane ND<25 Isopropylbenzene ND<25 <br /> Bromodichloromethane ND<25 p-Isopropyl toluene ND<25 <br /> Bromoform ND<25 Methyl butyl ketone' ' ND<25 <br /> Bromomethane ND<25 Methylene Chloride"' ND<85 <br /> n-Butyl benzene ND<25 Methyl ethyl ketone" ND<25 <br /> sec-Butyl benzene ND<25 Methyl isobuty)ketoneND<25 <br /> tert-Butyl benzene ND<25 Methyl tert-Butyl Ether(MTBE) <br /> Carbon Disulfide ND<25 Napthalene ND<60 <br /> Carbon Tetrachloride ND<25 n-Propyl benzene 36 <br /> Chlorohenzene ND<25 St,,rene' ' ND<25 <br /> C hloroethane ND<25 I 1 1 2-Tetrachloroethane ND<25 <br /> 2-Chloroethyl Vinyl Ether` ND<25 1 1 2 2-Tetrachloroethane ND<25 <br /> Chloroform ND<25 Tetrachloroethene ND<25 <br /> Chloromethane ND<25 Toluene" ND<25 <br /> 2-Chlorotoluene ND<25 1 2 3-Trichlorobenzene ND<25 <br /> 4-Chlorotoluene ND<25 1 2 4-Tnchlorobenzene ND<25 <br /> Dibromochioromethane ND<25 1 I 1 Trichloroethane ND<25 <br /> 12-Dibromo-3-chloropropane ND<25 1 12-Trichloroethane ND<25 <br /> Dibromomethane ND<25 Trichloroethene ND<25 <br /> 12-Dichlorobenzene ND<25 Tnchlorotluoromethane ND<25 <br /> 1,3-Dichlorobenzene ND<25 1 2 3-Tnchloropropane ND<25 <br /> 1,4-Dichlorobenzene ND<25 1 2 4-Tri methyl benzene 36 <br /> Dichlorodifluoromethane ND<25 1 3 5 Trimeth)lbenzene ND<25 <br /> 1,1-Di chlorocthane NTK25 Vinyl Acetate"" ND<25 <br /> 1 2-Dichloroethane ND<25 Vinyl Chloride"" ND<25 <br /> 1,1-Dichloroethene ND<25 Wenes total '° 46 <br /> cts-1,2-Dicbloroethene ND<25 <br /> trans-1,2-Dichloroethene ND<25 <br /> 1,2-Dichloropropane ND<25 <br /> 1 3-Dichloropropane N u<25 <br /> 2 2-Dichloropropane ND<25 Comments <br /> 1 1-Dichloropropene ND<25 Surrogate Recor eves(%) <br /> cis-) 3-Dichloropropene ND<25 Dibromot3uoromethane 112 <br /> trans-1,3-Dichloropropene ND<25 Toluene-d8 98 <br /> Ethylene dibromide ND<25 4-Bromofluorobenzene 115 <br /> water and vapor samples are reported in ug/L,sod and sludge samples in ug/kg w ipes in uglwtpe and a11 TCLP/SPLP extracts in ug/L <br /> Reporting limits unless Otherwise stated water samples 1 0 ug/L vapor samples 0 5 ug/L solid and sludge samples 5 ug/kg, wipes <br /> 0 2ugh ipe ND means not detected abo-,e the reporting limit NIA means analyte not applicable to this analysts <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy)ethene (d) 2-hexanone (e)dichloromethane (i) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present, (1)liquid sample that contains greater than —5 vol % <br /> sediment 0)sample diluted due to high organic content,(k)peaks present in this carbon range do not match the pattem of our standard fo <br /> this analyte,(1)methylbenzene(m)acetic acid ethenyl ester (n)chloroethene (o)dimethylbenzenes <br /> DHS Certification No 1644 'Edward Hamilton, Lab Director <br />