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I 10 Second Avenue South,#D7, Pacheco,CA 94553-5560 <br /> PMcCA,MPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 http//www mccampbell com E-mail main@mccampbell com <br /> EAdvanced GeoEnvironmentalClient Project ID Cal Fuels Date Sampled 07/16-07/17/98 <br /> Date Received 07/22/98 <br /> 4005 North Wilson Way <br /> l{ Stockton, CA 95205 Client Contact Tim Cuellar Date Extracted 07/29/98 <br /> Client P O Date Analyzed 07129-07/30/98 <br /> Volatile Organics By GCIMS <br /> EPA method 8260 <br /> Lab ID 92547 <br /> Client 1D MW2-7/17/98 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone" ND<600 Ethylbenzene 1700 <br /> Benzene 4800 }lexachlorobutadiene ND<250 <br /> Bromobenzene ND<250 lodomethane ND<250 <br /> Bromochloromethane ND<250 Isopropylbenzene ND<250 <br /> If Bromodichloromethane ND<250 p-Isopropyl toluene ND<250 <br /> Bromoform ND<250 Methyl butyl ketone' ' ND<250 <br /> Bromomethane ND--250 Methylene Chloride"' ND<850 <br /> n-Butyl benzene ND<250 Methyl ethyl ketone" ND<250 <br /> sec-Butyl benzene ND<250 Methyl isobutyl ketone'9 ND<250 <br /> ten-Butyl benzene ND<250 Methyl ten-Butyl Ether(MTBE) --- <br /> Carbon Disulfide ND<250 Napthalene ND<250 <br /> Carbon Tetrachloride ND<250 n-Propyl benzene ND<250 <br /> i Chlorobenzene ND<250 Styrene' ND<250 <br /> Chioroethane ND<250 1 1 1 2-Tetrachloroethane ND<250 <br /> 2-Chloroethyl Vinyl Ether" ND<250 1 1 2 2-Tetrachloroethane ND<250 <br /> C hloroform ND<250 Tetrachloroethene ND<250 <br /> Chloromethane ND<250 Toluene" 5100 <br /> 2-Chlorotoluene ND<250 1,2 3-Trtchlorobenzene ND<250 <br /> 4-Chlorotoluene NEX250 l 2 4-Trichloiabenzene ND<250 <br /> Dibromochloromethane ND<250 1 1 1 Trichloroethane ND<250 <br /> l2-Dibromo-3-chioropropane ND<250 1 12-Trichloioethane ND<250 <br /> Dibromomethane ND<250 Trichloroethene ND<250 <br /> 12-Dichiorobenzene ND<250 Trichlorofluoromethane ND<250 <br /> 1,3-Dichlarobenzene NDQ50 1,2,3-Tnchloropropane ND<250 <br /> i 4-Dichlorobenzene ND<250 1 2 4-Trimethyibenzene 1300 <br /> Dchlorodifluorometbanc ND<250 1 3 5-Trimethylbenzene 400 <br /> f 1 I-Dichloroethane ND<250 Vinyl Acetate""' ND<250 <br /> 1,2-Dichioroethane ND<250 Vinyl Chloride"" ND<250 <br /> I I-Dichloroethene NtX250 Xylenes total '"' 7500 <br /> cis-1 2-Dichloroethene ND<250 <br /> trans-l2-Dichloroethene ND<250 <br /> 1 2-Dichloronronane ND<250 <br /> 1 3-Dichloropropane ND<250 <br /> 2 2-Dichloropropane ND<250 Comments <br /> f 1 I-Dichloropropene ND<250 Surrogate RecoN cries <br />(` Cis-1,3-Diehl oropropene ND<250 Dibromofluoromethane 110 <br /> trans-l3-Dichloropropene ND<250 Toluene-d8 99 <br /> Ethylene dibmmide ND<250 4-Bromofluorobenzene 106 <br /> -,+.,ter and vapor samples are reported m ug/L sail and sludge samples in ug/kg,u,pes in ugk,tpe and all TCLP/SPLP extracts in ug/1_ <br /> Reporting limits unless otherwise stated water samples 10 ug/L vapor samples 0 5 ug/L, solid and sludge samples 5 ug/kg, wipes <br /> 0 2ug/wipe ND means not detected above the reporting limit,NIA means analyte not applicable to this analysts <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chioroethoxy)eihene, (d) 2-hexanone (e)dichloromethane (f) 2-butanone (g) 4-methyl-2- <br /> pentanone or isopropylaectone, (h)lighter than water immiscible sheen is present (i)liquid sample that contains greater than --5 vol % <br /> sediment 0)sample diluted due to high organic content,(k)peaks present in this carbon range do not match the pattem of our standard fo <br /> this analyte (1)methylbenzene;(m)acetic acid ethenyl ester (n)chloroethene (o)dimethylbenzenes <br /> DHS Certification No 1644 f/ Edward Hamilton, Lab Director <br /> i <br />