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I 10 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> h"flmccampbell com E-mail main@mccampbell com <br /> Advanced GeoEnvironmentalClient Project 1D Cal Fuels Date Sampled 07/16-07/17/98 <br /> Date Received 07/22/98 <br /> 4005 North Wilson Way <br /> Stockton,CA 95205 Client Contact Tim Cuellar Date Extracted 07/29/98 <br /> Client P O Date Analyzed 07/29-07/30198 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab 1D 92548 <br /> Client ID MW3-7/17/98 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone' ' ND<6500 Ethylbenzene 4100 <br /> Benzene 22,000 Hexachlorobutadiene ND<2000 <br /> Bromobenzene ND<2000 lodomethane N13<2000 <br /> Bromochioromethane ND<2000 I sopropyl benzene ND<2000 <br /> Bromodichloromethane ND<2000 p-Isopropyl toluene ND<2000 <br /> Bromoform ND<2000 Methyl butyl ketoneND<2000 <br /> Bromomethane ND<2000 Methylene Chloride" ND<7000 <br /> n-Butyl benzene ND<2000 Methyl ethyl ketone" ND<2000 <br /> sec-Butyl benzene ND<2000 Methyl isobutyl ketone'" ND<2000 <br /> tert-Butyl benzene ND<2000 Methyi tert-Butyl Ether(MTBE) -- <br /> Carbon Disulfide ND<2000 Napthalene ND<7500 <br /> Carbon Tetrachlonde ND<2000 n Propyl benzene N1X2000 <br /> 10 Chlorobenzene ND<2000 Styrene` ' ND<2000 <br /> Chloroethane ND<2000 1,1,1,2-Tetrachloroethane ND<2000 <br /> 2-Chloroethyl Vinyl Ether" ND<2000 1,1 2,2-Tetrachloroethane ND<2000 <br /> Chloroform ND<2000 Teirachloroethene ND<2000 <br /> Chloromethane ND<2000 Toluene" 17,000 <br /> 2-Chlorotoluene ND<2000 1,2,3-Trichloi obenzene ND<2000 <br /> 4-Chlorotoluene ND<2000 1 2 4-Trichloiobenzene ND<2000 <br /> Dibromochloromethane ND<2000 11 I-Trichloroethane ND<2000 <br /> 1,2-Dibromo-3-chloropropane ND<2000 112-Trichloroethane ND<2000 <br /> Dibromomethane ND<2000 Trichloroethene ND<2000 <br /> 12-Dichlorobenzene ND<2000 Trcchlorolluoromethane ND<2000 <br /> 1,3-Dichlorobenzene ND<2000 1 2,3-Trichloropropane ND<2000 <br /> 1,4-Dichlorobenzene ND<2000 1,2,4-Tnmethylben2ene 2500 <br /> Dichlorodifluoromethane ND<2000 1 3 5-Tnmethylbenzene ND<2000 <br /> 1,1-Dichloroeth2ne ND<2000 Vinyl Acetate""' ND<2000 <br /> 1 2-Dichioroethane ND<2000 Vinyl Chloride"" ND<2000 <br /> 1 1-Dichloroethene ND<2000 Xylenes total '°' 21,000 <br /> cis-1,2-Dichloroetbene ND<2000 <br /> trans-12-Dichloroethene ND<2000 <br /> 1 2-Dichloropropane ND<2000 <br /> 1 3-Dichloropropane ND<2000 <br /> 2 2-Dichloropropane ND<2000 Comments <br /> 1 1-Dichloropropene ND<2000 Surrogate Recos cries(%) <br /> cis-1,3-Dichloropropene ND<2000 Dibromotluoromethane 104 <br /> trans-1,3-Dichloropropene ND<2000 Toluene-d8 100 <br /> Ethylene dibromide I ND<2000 4 Bromotluorobenzene 103 <br /> water and vapor samples are reported in ug/LL,soil and sludge samples in ug/kg wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 0 ug/L ,apor samples 05 ug/L solid and sludge samples 5 ug/kg, wipes <br /> 0 Zug/wipe ND means not detected above the reporting limit N/A means analyte not applicable to this analysis <br /> (b) 2-prop2none or dtmethyl ketone, (c) (2-chloroethoxy)ethene (d) 2-hexanone (e)dichloromethane (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present, (i)liquid sample that contains greater than --5 vol % <br /> sediment,0)sample diluted due to high organic content,(k)peaks present in this carbon range do not match the pattern of our standard fo <br /> this analyte (1)methylbenzene:(m)acetic acid ethenyl ester,(n)chioroethi ne (o)dime ylbenzenes <br /> DHS Certificauon No 1644 / Edward Hamilton, Lab Director <br />