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110 Second Avenue South,#D7, Pacheco,CA 94553-5560 <br />' MCCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> t //www mccampbell com E-mail main@mccampbell com <br />' Advanced GeoEnvironmental Client Project ID Cal Fuels Date Sampled 07116-07/17/98 <br /> 4005 North Wilson Way <br /> Date Received 07/22/98 <br /> Stockton, CA 95205 Client Contact Tim Cuellar Date Extracted 07/29/98 <br /> Client P O Date Analyzed 07/29-07/30/98 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 92551 <br /> Client 1D MW6-7117198 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone ' ND<250 Ethylbenzene 150 <br /> Benzene 780 3-Iexachlorobutadiene ND<100 <br /> Bromobenzene ND<100 lodomelhane ND<100 <br /> Bromochloromcthane ND<100 lsopropylbenzetie ND<100 <br /> Bromodichloromethane ND<100 p-lsopropyl toluene NIX 100 <br /> Bromoform ND<100 Methyl butyl ketone' ' ND<100 <br /> Bromomethane ND<100 Methylene Chloride"' ND<250 <br /> n-Butyl benzene ND<l00 Methyl ethyl ketone" ND<100 <br /> sec-Butyl benzene N1X100 Methyl isobutyl ketone's ND<100 <br /> tent-Butyl benzene NIX100 Methyl tert-Butyl Ether(MTBE) --- <br /> Carbon Disulfide ND<100 Napthalene ND<100 <br /> Carbon Tetrachloride ND<100 n-Propyl benzene 110 <br /> Chlorobenzene ND<100 Styrene' ' N13<100 <br /> Chloroethane ND<100 1,1,1 2-Tetrachloroethane ND<100 <br /> 2-Clilorcethyl Vinyl Ether"I ND<100 1 1,2 2-Tetrachloroethane ND<]00 <br /> Chloroform ND<100 Tetrachloroethene ND<100 <br /> Chloromethane ND<100 Toluene" ND<100 <br /> 2-Chlorotoluene NDa100 1 2 3-Trichloiobenzene ND<100 <br /> 4 Chlorotoluene ND<100 1 2 4-Trichlorobenzene N13<100 <br /> Dibromochloromethane ND<100 I 1 I-Trichloroethane ND<100 <br /> l2-Dibromo-3-chloropropane ND<100 t,12-Trichloroethane ND<100 <br /> Dibromomethane ND<100 Tnehloroethene ND<!00 <br /> 12-Dichlorobenzene ND<100 Trichlorofluoromethane ND<100 <br /> 13-Dichlorobenzene NIX100 1 2 3-Tnchloropropane NIX100 <br /> 1,4-Dichlorobenzene ND<100 1 2 4-Trimethy]benzene 220 <br /> Dichlorodifluoromethane ND<100 1,3 5-Trimethylbenzene ND<100 <br /> 1,1-Dichloroethane ND<100 Vinyl Acetate""' ND<100 <br /> 1,2-Dichloroethane ND<100 Vinyl Chloride"" ND<100 <br /> 1,1-Diehl oroethene ND<]00 Xylenes,total `°' ND<100 <br /> cis-1 2-Dichloroethene ND<100 <br /> trans-1,2-Dichloroethene ND<100 <br /> 12-Dichloropropane NUc100 <br /> 13-Dichloropropane ND<100 <br /> 2,2-Dichloropropane ND<100 Comments <br /> 1,1-Dichloropropene ND<100 Surrogate Recoi cries(%) <br /> cis-l3-Dichloropropene ND<100 Dibromotluoromeihane 107 <br /> trans-] 3-Dichloropropene ND<100 Toluene-d8 102 <br /> Ethylene dibromide ND<100 4-Bromofluorobenzene 126 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 0 ug/L, 1,apor samples 05 ug/L solid and sludge samples 5 ug/kg, wipes <br /> 0 2ug/%%ipe ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present (i)liquid sample that contains greater than--5 vol 0/0 <br /> li sediment 0)sample diluted due to high organic content (k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte,(1)methylbenzene,(m)acetic acid ethenyl ester,(n)chloroethene (o)dimethylbenzenes <br /> DHS Certification No 1644 //,-'—Edward Hamilton, Lab Director <br />