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I 10 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//wwm <br /> w ccampbell corn E-mail math@mccampbell corn <br /> Date Sampled 07/16-07117/98 <br /> Advanced GeoEnvironmental Client Project ID Cal Fuels <br /> 4005 North Wilson Way <br /> Date Received 07/22/98 <br /> f <br /> Stockton, CA 95205 Client Contact Tim Cuellar Date Extracted 07/29/98 <br /> Client P O Date Analyzed 07/29-07130198 <br /> Volatile Organics By GC/MS <br /> EPA method 8200 <br /> Lab ID 92552 <br /> Client ID MW7-7!17/98 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone" ND<3 Ethylbenzene ND <br /> Benzene ND Hexachlorobutadiene ND <br /> Bromobenzene ND lodomethane ND <br /> Bromochloromethane ND Isopropylbenzene ND <br /> Bromodichloromethane ND p-lsopropyl toluene ND <br /> Bromoform ND Methyl butyl ketone' ' ND <br /> Bromomethane ND Methylene Chloride"' ND <br /> n-Butyl benzene ND Methyl ethyl ketone' ND <br /> sec-Butyl benzene ND Methyl isobutyl ketone`" ND <br /> tert-Butyl benzene ND Methyl ten-Bulyl Ether(MTBE) --- <br /> Carbon Disulfide ND Napthalene ND <br /> Carbon Tetrachloride ND n-Propyl benzene ND <br /> Ch€orobenzene ND Styrene' ' ND <br /> Chloroethane ND 1 1,12-Tetrachloroethane ND <br /> 2-Chloroethyl Vinyl Ether" ND 1,1 2 2-Tetrachloroethane ND <br /> C hlorotorm ND Tetrachloroethene ND <br /> Chloromethane ND Toluene"' ND <br /> 2-Chlorotoluene ND 123-Trich€orobenzene ND <br /> 4-C hlorotoluene ND 1 2 4-Trichloroben2e11e ND <br /> Dibromochloromethane ND 11 1-Trichloroethane ND <br /> 12-Dibromo-3-chloropropane ND 112-Trichloroethane ND <br /> Dibromomethane ND Trichloroethene ND <br /> 1 2-Dichlorobenzene ND TrichlOM11U01omethane ND <br /> 1 3-Dichlorobenzene ND 1 2 3-Trichloroprop3ne ND <br /> 1 4-Dichlorobenzene ND 1 2 4-Trimethylbenzene ND <br /> Dichlorodifluoromethane ND 1 3 5-Trimethylbenzene ND <br /> 1 1-Dichloroethane ND Vinyl Acetate"'I ND <br /> 12-Dichloroethane ND Vinyl Chloride"" ND <br /> l,I-Dichloroethene ND Xylenes total '°' ND <br /> cis-1 2-Dichloroethene ND <br /> trans-1 2-Dichloroethene ND <br /> 1,2-Dichloropropene ND <br /> i 3-Dicmoropropane NU <br /> 2 2-Diehl oropropane ND Comments <br /> 1 1-Dichloropropene ND Surrogate Reco%cries(%) <br /> cis-1,3-Dichloropropene ND Dibromolluoromethane 110 <br /> trans-],3-Dichloropropene ND Toluene-d8 99 <br /> Ethylene dibromtde ND 4-Bromolluorobenzene 105 <br /> Hater and vapor samples are reported to ug/L,soil and sludge samples in ug/kg,Hipes in ughtiipe and all TCLP I SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 0 ug/L, vapor samples 0 5 ug/L solid and sludge samples 5 ug/kg, wipes <br /> 0 Zug/wipe ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy)ethene (d) 2-hexanone, (e)dichloromethane (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropyl acetone, (h)lighter than water immiscible sheen is present (i)liquid sample that contains greater than —5 vol % <br /> sediment 0)sample diluted due to high organic content,(k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte,(1)methylbenzene;(m)acetic acid ethenyl ester,(n)chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 -2 Edward Hamilton,Lab Director <br />