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I 10 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax:925-798-1622 <br /> hq://www.mceMpbeil.com E-mail:main@mecampbell.com <br /> V <br /> / <br /> 10/29 <br /> -3001 i <br /> Advanced GeoEnvironmental Client Project ID: Cal Fuels Date Sampled: � <br /> 837 Shaw Road Date Received: 10/31/01 f <br /> t. <br /> Stockton, CA 95215 Client Contact:Tim Cuellar Date Extracted: 11/03/01 <br /> Client P.O: Date Analyzed: 11/03/01 <br /> Volatile Organics By GUMS <br /> EFA method 8260 <br /> Lab ID 82296 <br /> Client ID CPT2A/106-115 <br /> Matrix W <br /> * Reporting Limit Reporting Limit <br /> Compound Concentration W S Compound Concentration* <br /> W S <br /> Acetone(t) ND 5A 25 trans-l,3-Dichloropropene ND 1.0 5.0 <br /> Lo Benzene 15 1.0 5.0 Ethylene dibromide ND 1.0 5.0 <br /> Bromobenzene ND 1.0 5.0 Ethylbenzene 21 1.0 5.0 <br /> Bromochloromethane ND 1.0 5.0 Hcxachlorobutadiene ND 5.0 25 <br /> Bromodichloromethanc ND Lo 5.0 Iodomethane ND L0 5.0 <br /> �" Bromoform ND LO 5.0 Iso ro lbenzene <br /> P PY 1.8 1.0 5.0 <br /> Bromomethane ND 1.0 5.0 p-Isopropyl toluene ND 1.0 5.0 <br /> n-Butyl benzene 2.0 1.0 5.0 Methyl butyl ketone' ND 1.0 5.0 <br /> V sec-Butyl benzene ND 1.0 5.0 Methylene Chlorides` ND 1.0 5.0 <br /> tert-Butyl benzene ND 1.0 5.0 1 Methyl ethyl ketone' ND 2.0 lD <br /> Carbon Disulfide ND 1.0 5.0 Methyl isobutyl ketone ND 1.0 5.0 <br /> Carbon Tetrachioride ND 1.0 5.0 Methyl tent-Butyl Ether(MTBE) - I.0 5.0 <br /> i.. Chlorobenzeue ND Lo 5.0 Naphthaiene ND 5.0 5.0 <br /> Chloroethane ND LO 5.0 n-Propyi benzene 6.6 1.0 5.0 <br /> 2-Chioroethyl Vinyi Ether` ND- 1.0 5.0 Styrene ND 1.0 5.0 <br /> Chloroform ND 1.0 5.0 1,1,1,2-Tetrachloroethane ND LO 5.0 <br /> Chloromethane ND 1.0 5.0 1,1,2,2-Tetrachloroethane ND LO 5.0 <br /> 2-Chlorotoluene ND 1.0 5,0 Tetrachloroethene ND 1.0 5.0 <br /> 4-Chlorotoluene ND 1.0 5.0 Toluene 72 1,0 5.0 <br /> Dibromochloromethane ND 1.0 5.0 1,2,3-Trichlorobenzene ND 5.0 25 <br /> La 1,2-Dibromo-3-chloropropane ND 2.0 10 1,2,4-Trichlorobenzene ND 5.0 25 <br /> Dibromomethane ND 1.0 5.0 1,1,1-Trichloroethane ND 1.0 5.0 <br /> 12-Dichlorobenzene ND 1.0 5.4 1,1,2-Trichloroethane ND 1.0 5.0 <br /> 1,3-Dichlorobenzene ND 1.0 5.0 Trichloroethene ND 1.0 5.0 <br /> iL. 1,4-Dichlorobenzene ND 1.0 5.0 Trichlorofluoromethane ND 1.0 5.0 <br /> Dichlorodifluoromethane ND 1.0 5.0 1,2,34richloropropane ND 1.0 5.0 <br /> 1,1-Dichloroethane ND 1.0 5.0 1,2,4-Trimethylbenzene 33 1.0 5.0 <br /> 1,2-Dichloroethane ND 1.0 5.0 1,3,5-Trimethylbenzene 1.8 1.0 5.0 <br /> 1,1-Dichloroethene ND 1.0 5.0 Vinyl Acetate ND 5.0 25 <br /> cis-1,2-Di chloroethene ND 1.0 5.0 Vinyl Chloride(n) ND 1.0 5.0 <br /> trans-l,2-Dichloroethene ND 1.0 5.0 Xylenes,total 97 1.0 5.0 <br /> 1,2-Dichloropropane ND 1.0 5.0 Comments: <br /> L.. 1,3-Dichloropropane ND l.0 5.0 1 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 1.0 5.0 Dibromofiuoromethane 106 <br /> 1,1-Dichloropropene ND 1.0 5.0 Toluene-d8 99 <br /> cis-1,3-Dichloropropene ND 1.0 5.0 4-Bromotluorobenzene 96 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit;NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (t) 2-butanone; (g) 4-methyl-2- <br /> La pentanone or isopropylacetone; (h)lighter than water immiscible sheen is present; (i)liquid sample that contains greater than-5 vol. % <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; 0) methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> / chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br /> La <br />