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w.. <br /> 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC, Telephone: 925-798-1620 Fax : 925-798-1622 <br /> htt�//www.mccMbell.com E-mail:main@mccampbell.com <br /> i. <br /> Advanced GeoEnvironmental Client Project ID:Cal Fuels Date Sampled: 10/29-30/01 <br /> 837 Shaw Road Date Received: 10/31/01 <br /> r«. <br /> Stockton, CA 95215 Client Contact: Tim Cuellar Date Extracted: 11/03-11/07/01 <br /> Client P.O: Date Analyzed: 11/03-11107101 <br /> E <br /> EPA method 8260 Volatile Organics By GC/MS <br /> Lab ID 82297 <br /> Client ID CPT2A/121-125 <br /> i„ Matrix yit <br /> * Reporting Limit Repotting Limit <br /> Compound Concentration W S Compound Concentration* <br /> W S <br /> Acetone @} N0<€0 1215 trans-1,3-Dichloropropene ND 1.0 5.0 <br /> �" Benzene 10 .0 Ethylene dibromide ND 1.0 5.0 <br /> Bromobenzene ND 0 Ethylbenzene 14 1.0 5.0 <br /> Bromochloromethane ND A Hexachlorobutadiene ND 5.0 25 <br /> Bromodichioromethane ND .0 Iodomethane ND 1.0 5.0 <br /> Bromofotrn ND .D Isopropylbenzene 1.1 1.0 5.0 <br /> Bromomethane ND .D p-Isopropyl toluene Nil Lo 5.0 <br /> n-Butyi benzene ND 0 Methyl butyl ketone ND 1.0 5.0 <br /> sec-Butyl benzene ND 0 Methylene Chloride` ND 1.0 5.0 <br /> Wtert-Butyl benzene ND 0 Methyl ethyl ketone ND 2.0 10 <br /> Carbon Disulfide ND 0 Methyl isobutyl ketone ND 1.0 5.0 <br /> Carbon Tetrachloride ND . .0 Methyl tert-Butyl Ether(MTBE) --- 1.0 5.0 <br /> r Cblorobenzene ND 1.0 5.0 Naphthalene 11 5.0 5.0 <br /> Chloroethane ND 1.0 5.0 n-Propyl benzene 4.4 Lo 5.0 <br /> 2-Cbloroethyl Vinyl 8tber ND 1.0 5.0 Styrene ND LO 5.0 <br /> Chloroform ND 1.0 5.0 1,1,1,2-Tetrachloroethane ND 1.0 5.0 <br /> W Chioromethane ND 1.0 5.0 1,1,2.,2-Tetrachloroethane ND 1.0 5.0 <br /> 2-Chlorotoluene ND 1.0 5.0 Tetrachloroethene ND 1.0 5.0 <br /> 4-Chlorotoluene ND 1.0 5.0 Toluene{ 52 1.0 5.0 <br /> Dibromochloromethane ND 110 5.0 1,2,3-Trichlorobenzene ND 5.0 25 <br /> LM 1,2-Dibromo-3-chloropropane ND 2.0 10 1,2,4-Trichlorobenzene ND 5.0 25 <br /> Dibromomethane ND LO 5.0 1,1,1-Trichloroethane ND 1.0 5.0 <br /> 1,2-Dichlorobenzene ND 1.0 5.0 1,1,2-Trichloroethane ND 1.0 5.0 <br /> 1,3-Dichlorobenzene ND lA 5.0 Trichloroethene ND 1.0 5.0 <br /> &W 1,4-Dichlorobenzene ND 1.0 5.0 Trichlorofluoromethane ND 1.0 5.0 <br /> Diehiorodifluoromethanc ND 1.0 5.0 1,2,3-Trichloroprapane ND 1.0 5.0 <br /> 1,1-Dichioroethane ND 1.0 5.0 1,2,4-Trimethyibenzene 32 1.0 5.0 <br /> 1,2-Dichloroethane ND 1.0 5.0 1,3,5-Trimethylbenzene 9.1 €.0 5.0 <br /> i.. 1,1-Dichloroethene ND 1.0 5.0 Vinyl Acetate t'° ND 5.0 25 <br /> cis-1,2-Dichloroethene ND 1.0 5.0 Vinyl Chloride n' ND 1.0 5.0 <br /> trans-€,2-Dichloroethene ND 1.0 5.0 Xylenes,total 73 1.0 5.0 <br /> 1,2-Dichioropropane ND 1.0 5.0 Comments: <br /> Lo 1,3-Dichloropropane ND 1.0 5.0 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 1.0 5.0 Dibromofluoromethane 107 <br /> 1,1-Dichloropropene ND 1.0 5.0 Toluene-d8 100 <br /> cis-1,3-Dichloropropene ND 1.0 5.0 4-13romofluorobenzene 99 <br /> LN <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP 1 SPLP extracts in ug/L <br /> ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis <br /> (h) 2-propanone or dimethyl ketone; (c) (2-chloroetboxy) ethene; (d) 2-hexanone; (e) dichloromethane; (f) 2-butanone; (g) 4-methyl-2- <br /> pentanone or isopropyiacetone; (h)lighter than water immiscible sheen is present; (i)liquid sample that contains greater than-5 vol. % <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; (1) methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> �✓ chloroethene;(o)dimethylbenzenes. 10 <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br /> L <br />