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CASTLE ANALYTICAL LABORATORY <br /> Environmental Testing Services 2333 Shuttle Drive,Atwater,CA 95301 Phone (209)384-2930 <br />' Certificate#2480 Fax (209)384-1507 <br /> F <br /> Environmental, Inc Client Project ID Cal-Fuels Sampled 12-31-02 <br /> lifornia Reference Number 5359 Received 01-03-03 <br /> d Sample Description Water Extracted 01-06-03 <br /> 5215 Sample Prep/Analysis Method EPA 5030/8015 8020 Analyzed 01-06-03 <br /> ar Lab Numbers 5359-11W, 12W, 13W Reported 01-10-03 <br />' TOTAL PETROLEUM HYDROCARBONS -GASOLINE <br /> WITH BTEX DISTINCTION <br />' ANALYTE REPORTING LIMIT SAMPLE 1D SAMPLE ID SAMPLE ID <br /> AW 1 B AW 2A AW 2B <br /> 12-31-02 12-31-02 12-31-02 <br /> 1 (ug/L) (ug/L) (ug/L) (ug/L) <br /> MTBE 050 ND ND ND <br /> BENZENE 050 760 6800 2800 <br /> TOLUENE 050 210 33000 20000 <br /> ETHYLBENZENE 050 1500 3800 2200 <br />' TOTAL XYLENES 050 5100 19000 9200 <br />' GASOLINE RANGE <br /> HYDROCARBONS 50 31000 130000 52000 <br /> Report Limit Multiplication Factor 100 1000 500 <br /> I <br /> Surrogate%Recovery FID 125%JPI1) 110% FID 105%/PID 103% RD IM)PID 106% <br /> Instrument ID VAR-GC1 VAR-GC1 VAR-GC1 <br /> Analytes reported as ND were not detected or below the Practical Quantitation Limit <br /> Practical Quantitation Limit= Reporting Limit x Report Limit Multiplication Factor <br /> ANALYST /• APPROVED BY <br /> Clan Cone Ja hdlrps <br /> Iboratory Director <br />