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' CASTLE ANALYTICAL <br /> . LABORATORY <br /> Environmental Testing Services 2333 Shuttle Drive,Atwater, CA 95301 Phone (209) 384-2930 <br /> Certificate No 2480 Fax (209)384-1507 <br /> Advanced Geo Environmental Inc Client Project ID Ca!-Fuels Sampled 12-31-02 <br />' of Northern California Reference Number 5359 Received 01-03-02 <br /> 837 Shaw Road Sample Description Water Extracted 01-06-02 <br /> Stockton CA 95215 Sample Prep/Analysis Method EPA 5030/8260 Analyzed 01-06-02 <br /> Atte Tim Cuellar Lab Numbers 5359-1W,2W 3W,4W 5W Reported 01-10-02 <br /> GASOLINE ADDITIVES BY EPA METHOD 8260 GUMS <br /> ANALYTE REPORTING SAMPLE ID SAMPLE 1D SAMPLE ID SAMPLE ID SAMPLE ID <br />' LIMIT MW 1 MW 2 MW 3 MW 6 MW 10 <br /> 12-31-02 12-31-02 12-31-02 12-31-02 12-31-02 <br /> p /L {u IL (u /L) (u/L (ug/L} u /L) <br />' <br /> FUEL,OXYGENATES <br /> Methyl tert-Butyl Ether(MTBE) 050 ND ND ND ND NO <br /> Di-isopropyl Ether (DIPE) 050 ND ND ND ND ND <br /> Ethyl tert-Butyl Ether (ETRE) 050 ND NO ND ND ND <br /> tert-Amyl Methyl Ether(TAME) 050 ND ND NO NO ND <br /> tert-Butanol(TBA) 20 NO ND ND ND ND <br /> VOLATILE HALOCARBONS <br /> 1 2-Dichloroothane 0 2-DCA) 050 ND ND ND ND ND <br /> Ethylene Dibromide (EDB) 050 NO ND ND ND ND <br /> Report Limit Multiplication Factor 1 1 20' 1 1 <br /> "Report limit raised due to matrix interference <br /> 1 2-Dichloroethane-d4 869% 106% 101% 999% 844% <br /> Toluene-d8 106% 102% 105% 102% 102% <br /> Instrument ID HP 5972 MS <br /> Analytes reported as ND were not detected or below the Practical Quantitation Limit <br /> Practical Quantitation Limit= Reporting Lima x Report Limit Multiplication Factor <br /> (Ng/L)= micrograms per liter or parts per billion (ppb) <br /> ANALYST APPROVED BY <br /> Clan Cone Ja s hillips <br /> Iboratory Director <br /> I <br />