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' CASTLE <br /> ANALYTICAL LABORATORY <br /> ' Environmental Testing Services 2333 Shuttle Drive,Atwater CA 95301 Phone (209)384-2930 <br /> Certificate No 2480 Fax (209)384-1507 <br /> F <br /> ced GeoEnvironmental Inc Client Project ID Cal-Fuels Sampled 12-30-02 <br /> hern California Reference Number 5354 Received 12-31-02 <br /> aw Road Sample Descnption WaterExtracted D1-02-03 <br /> on, CA 95215 Sample Prep/Analysis Method EPA 5030/8260 Analyzed 01-02-03 <br /> im Cuellar Lab Numbers 5354-6W Reported 01-06-03 <br /> 1 <br />' GASOLINE ADDITIVES 6Y EPA METHOD 8260 GC1MS <br /> ANALYTE REPORTING SAMPLE ID <br />' LIMIT Mw- 11 <br /> 12-30-02 <br /> IL u /L <br />' FUEL XYGENATES <br /> Methyl tert-Butyl Ether(MTBE) 050 ND <br />' Dr-isopropyl Ether (DIPE) 050 ND <br /> Ethyl tert-Butyl Ether (ETBE) 050 ND <br />' tert-Amyl Methyl Ether(TAME) 050 ND <br /> tert-Butanol(TBA) 20 ND <br />' VOLATILE HAL CAR ON <br /> 1 2-Dichloroethane (1,2-DCA) 050 ND <br />' Ethylene Dibromide (EDB) 050 ND <br />' Report Limit Multiplication Factor 1 <br /> I <br /> Surrogate Recoveries <br /> 1,2-Dichloroethane-d4 934% <br /> Toluene-d8 101% <br /> Instrument ID Varian Saturn 3 MS&HP 5972 MS <br /> Analytes reported as ND were not detected or below the Practical Quantitation Limit <br /> Practical Quantitation Limit=Reporting Limit x Report Limit Multiplication Factor <br /> (pg/L)= microgramsperliter or parts bill n(ppb) <br /> r <br /> 7 <br /> ANALYST APPROVED BY <br /> Clary J Con Ja Phillips <br /> / boratary Director <br /> 1 <br />