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' CASTLE ANALYTICAL LABORATORY <br /> Environmental Testing Services 2333 Shuttle Drive,Atwater,CA 95301 Phone (209)384-2930 <br />' Certificate No 2480 Fax (209)384-1507 <br /> FFAdvanced GeoEnvironmental Inc Client Protect ID Cal-Fuels Sampled 12-31-02 <br />' rthern California Reference Number 5359 Received 01-03-02 <br /> 837 Shaw Road Sample Description Water Extracted 01-06-02 <br /> Stockton, CA 95215 Sample Prep/Analysis Method EPA 5030/8260 Analyzed 01-06-02 <br /> Attn Tim Cuellar Lab Numbers 535"W,7W, BW, 9W, 10W Reported 01-10-02 <br /> 1 <br /> GASOLINE ADDITIVES BY EPA METHOD 8260 GCIMS <br /> 1 <br /> ANALYTE REPORTING SAMPLE ID SAMPLE ID SAMPLE ID SAMPLE ID SAMPLE ID <br />' LIMIT MW 12 MW 13A MW 13B MW 13C AW 1A <br /> 12-31-02 12-31-02 12-31-02 12-31-02 12-31-02 <br /> _ funic) (uq/L) (ug/L)_ _(uglL) _ _ (ug/L) <br />' EIIEL OXYGENATES <br /> Methyl tert-Butyl Ether(MTBE) 050 ND NO NO NO NO <br /> Di-isopropyl Ether (RIPE) 050 NO ND NO NO NO <br /> Ethyi tert-Butyl Ether (ETRE) 050 ND NO NO ND ND <br /> lietert-Amyl Methyl Ether(TAME) 050 ND ND ND ND NO <br /> tert-Butanol(TBA) 20 ND ND NO ND NO <br />' VQLATILE HALQCARBONS <br /> 1 2-Dichioroethane (1 2-DCA) 050 NO NO NO ND NO <br />' Ethylene Dibromide (EDB) 050 NO NO ND ND NO <br />' Report Limit Multiplication Factor 1 1 1 1 20" <br /> "Report limit raised due to matrix interference <br /> vrerie3 <br /> 1,2-Dichloroethane-d4 967% 864% 923% 983% 916% <br /> Toluene-d8 102% 105% 983% 994% 106% <br /> Instrument ID HP 5972 MS <br /> Analytes reported as NO were not detected or below the Practical Quantitation Limit <br /> Practical Quantitation Limit=Reporting Limit x Report Limit Multiplication Factor <br /> (Ng/L)= micrograms per liter or parts per billion(ppb) <br /> ANALYST <br /> � APPROVED BY <br /> Clan J Cone r es C Phrllrps <br /> Laboratory Director <br />