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1 7 Analytical 1 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCampbell Aytical Inc. Telephone:925-798-1620 Fax:925-798-1622 <br /> A# http://www.mccarnpbell.com E-mail:main@mccampbell.com <br /> Advanced GeoEnvironmental,Inc Client Project ID: Cal Fuels Date Sampled: 09/20/02 <br /> 837 Shaw Road Date Received: 09/24/02. <br /> Client Contact: Tim Cuellar Date Extracted: 09/27/02 <br /> Stockton,CA 95215 <br /> Client P.O.: Date Analyzed: 09/27/02 <br /> Oxygenated Volatile Organics+EDB and 1,2-DCA by P&T and GC/MS* <br /> jj Extraction Method: SW5030B Analytical Method:SW8260B Work Order:0209369 <br /> f x Lab 1D 0209369-005B 0209369-0068 0209369-007B 0209369-0088 <br /> { � Client ID MW5/092002 MW61092002 MW71092002 ' MW8/092002 Reporting Lint for <br /> Matrix W W W W <br /> DF=l <br /> S. W <br /> 1 i <br /> Compound Concentration ug/kg µglL <br /> f � <br /> Diisopropyl ether(DIPE) ND ND ND ND NA 0.5 <br /> # 1 Ethyl tert-butyl ether(E.TBE) ND ND ND ND NA 0.5 <br /> Methyl-t-butyl ether(MTBE) 0.64 ND ND i ND NA 0.5 <br /> tett-Amyl methyl ether(TAME) ND ND ND � ND NA 0.5 <br /> n <br /> t-Butyl alcohol(TBA) ND ND I ND ND NA 5.0 <br /> t <br /> 1,2-Dibromoetham(EDB) ND ND ND ND NA 0.5 <br /> 1 <br /> 1,2-Dichloroethane(1,2-DCA) 1.5 ND ND ND NA 0.5 <br /> I <br /> Surrogate Recoveries(%) <br /> 99.8 97.7 99.5 98.4 <br /> Comments <br /> *water and vapor samples and all TCLP&SPLP extracts are reported in ug/L,soil/sludge/solid samples in ug/kg, wipe samples in ug/wipe, <br /> d product/oWrion-aqueous liquid samples in mg/L. <br /> ND means not detected above the reporting limit;NIA means analyte not applicable to this analysis. <br /> h)lighter than water immiscible sheen/product is present;i)liquid sample that contains greater than—2 vol.%sediment;j)sample diluted due to high <br /> organic content. <br /> l <br /> y <br /> i <br /> i <br /> DH Certification No. 1644 Edward Hamilton <br /> SC o � ,Lab Director <br /> ............., ... . ,.� <br />