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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCampbell Analytical Inc. Telephone:925-798-1620 Fax:925-798-1622 <br /> http://www.mccamphell.corn E-mail:maitt@mccampbell.com <br /> Advanced GeoEnvironmental,Inc Client Project ID: Cal Fuels Date Sampled: 09/20/02 <br /> 837 Shaw Road Date Received: 09/24/02 <br /> Client Contact: Tim Cuellar Date Extracted: 09/27/02 <br /> Stockton, CA 95215 <br /> [Client P-O.: Date Analyzed: 09/27/02 <br /> Oxygenated Volatile Organics+EDS and 1,2-DCA by P&T and GC/MS* <br /> Extraction Method: SW5030B Analytical Method:SW8260B Work Order:0209369 <br /> Lab ID 0209369-009B 10209369-OIOB 0209369-011B 0209369-012B <br /> +� Client ID MW9/092002 MW10/092002 MW11/092002 MW12/092002 <br /> Reporting Limit for <br /> Matrix W W W W DF=l <br /> S W <br /> Compound Concentration ug/kg Pg/L <br /> I <br /> i <br /> Diisopropyl ether(DIPE) ND ND ND ND NA 0-5 <br /> Ethyl tert-butyl ether(ETRE) ND ND ND I ND NA 0.5 <br /> i <br /> i <br /> Methyl-t-butyl ether(MTBE) ND ND ND ! ND NA 0.5 <br /> i <br /> i <br /> tert-Amyl methyl ether(TAME) ND ND NDND NA 0.5 <br /> i <br /> y t-Butyl alcohol(TBA) ND ND ND ND NA 5.0 <br /> 1,2-Dibromoethane(EDB) ND ND ND ND NA 0.5 <br /> 1,2-Dichloroethane(1,2-DCA) ND ND ND 1 ND NA 0.5 <br /> 'I <br /> Surrogate Recoveries(%) <br /> �+ %SS; 97-6 48.0 98.5 98.5 <br /> Comments <br /> ++ *water and vapor samples and all TCLP&SPLP extracts are reported in ug/L,soil/sludge/solid samples in ug/kg, wipe samples in uglwipc, <br /> product/oil/non-aqueous liquid samples in mg/L. <br /> ND means not detected above the reporting limit;NIA means analyte not applicable to this analysis. <br /> h)lighter than water immiscible sheen/product is present;i)liquid sample that contains greater than—2 vol.%sediment;j)sample diluted due to high <br /> organic content. <br /> r <br /> V <br /> Sim <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br />