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1.. 110 2nd Avenue South,#D7,Pacheco,CA 94553.5560 <br /> McCampbell Analytical Inc. Telephone:925-798-1620 Fax:925-798.1622 <br /> http:llwww.mccampbell.com E-mail:main®mccampbell.com <br /> Advanced GeoEnvironmental,Inc Client Project ID: Cal Fuels Date Sampled: 09/20/02 <br /> 837 Shaw Road <br /> Date Received: 09/24/02 <br /> Client Contact: Tim Cuellar Date Extracted: 09/27/02 <br /> ++ Stockton,CA 95215 <br /> Client P.O.: Date Analyzed: 09/27/02 <br /> Oxygenated Volatile Organics f EDB and 1,2-DCA by P&T and GCIMS* <br /> Fxuaction Method: SW5030B Analytical Method:SW8260B Work Order:0209369 <br /> Lab ID 0209369-013B 0209369-0148 0209369-015B l 0209369-016B <br /> ClientlD AW1A/092002 AWIB/092002 I AW2A1092002 AW2B/092002 <br /> Reporting Limit for <br /> Matrix W W W W DF=t <br /> +� DF 10 10 10 ! 10 <br /> 5 W <br /> Compound Concentration ug/kg µg/L <br /> Diisopropyl ether(DIPS.) ND<5.0 N1<5.0 ND<5.0 ND<5.0 NA0.5 <br /> Ethyl tert-butyl ether(ETBE) ND<5.0 ND<5.0 ND<5.0 ND<5.0 NA 0.5 <br /> �+ E <br /> Methyl-t-butyl ether(MTBE) ND<5.0 ND<5.0 ND<5.0 ND<5.0 NA 0.5 <br /> tert-Amyl methyl ether(TAME) ND<5.0 ND<5.0 ND<5.0 ND<5.0 NA T 0-5 <br /> .-. t-Butyl alcohol(TBA) ND<50 ND<50 ND<50 ND<50 NA 5.0 <br /> 1,2-Dibromoethane(EDB) ND<5.0 ND<5.0 I ND<5.0 ND<5.0 NA 0.5 <br /> i <br /> 1,2-Dichloroethane(1,2-DCA) ND<5.0 ND<5.0 ND<5.0 30 NA 0.5 <br /> I c <br /> Surrogate Recoveries{%) <br /> +�+ °/aSS: 95.6 97.8 98.8 99.3 <br /> Comments j <br /> � I <br /> s+ *water and vapor samples and all TCLP&SPLP extracts are reported in ug/L,soil/sludge/solid samples in ug/kg, wipe samples in ug/wipe, <br /> product/oil/non-aqueous liquid samples in mg/L. <br /> ND means not detected above the reporting limit;NIA means analyte not applicable to this analysis. <br /> rr <br /> h)lighter than water immiscible sheen/product is present;i)liquid sample that contains greater than-2 vol.%sediment;j)sample diluted due to high <br /> organic content. <br /> LW <br /> r <br /> r � <br /> S- . <br /> r <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br />