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' 110 2nd Avenue South #1)7 Pacheco CA 94553 5560 <br /> McCatnpbell Analytical Inc Telephone 925-798-1620 Eax 925-798-1622 <br />' http//www mcca bell com E mail maul mecampbell cam <br /> Advanced GeoEnvironmental,Inc Client Project ID (Arco)Pacific Mini Date Sampled 02/25/03 <br /> Mart <br />' 837 Shaw Road Date Received 02/27/03 <br /> Client Contact Bill Little Date Extracted 03/01/03-03/05/03 <br /> Stockton, CA 95215 <br />' Client P O Date Analyzed 03/01/03-03105/03 <br /> Oxygenates and BTEX by GC/MS* <br /> Extraction Method SW5030B Analytical Method SW8260B Work Order 0302377 <br />' Lab ID 0302377-OOIB 0302377-002B 0302377-003B 0302377-004B <br /> Client ID MW 1 MW 2 - -- MW 3 MW 4 Reporting Limit for <br /> Matrix W W — W W <br /> DF 1 1 1 20 S }N <br /> 1 Compound Concentration ug/kg El <br /> tert-Amyl methyl ether(TAME) ND ND ND ND<10 NA 05 <br />' Benzene ND ND ND 250 NA 0 5 <br /> t-Butyl alcohol(TBA) ND ND ND ND<100 NA 5 0 <br />' 1,2-Dibromoethane(EDB) ND ND ND ND<10 NA 0 5 <br /> 1,2-Dichloroethane(1 2-DCA) ND 0 54 0 91 ND<10 NA 0 5 <br /> Dusopropyi ether(DIPE) ND ND ND ND<10 NA 0 5 <br /> lie <br /> Ethylbenzene ND ND ND 610 NA 0 5 <br /> Ethyl tert-butyl ether(ETBE) ND ND ND ND<10 NA 05 <br />' Methyl-t-butyl ether(MTBE) ND 7 1 96 400 NA 0 5 <br /> Toluene ND ND ND 18 NA 0 5 <br />' Xylenes – ND ND ND 620 NA 0 5 <br /> Surrogate Recoveries(%) <br />' %SS1 118 114 119 116 <br /> %SS2 110 107 109 110 <br /> %SS3 98 0 94 3 977 91 1 <br /> Comments <br /> *water and vapor samples and all TCLP&SPLP extracts are reported in gg/L,soil/sludge/solid samples inµg/kg, wipe samples in Ag/wtpe, <br /> product/oillnon-aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> h)lighter than water immiscible sheen/product is present,1)liquid sample that contains greater than—2 vol %sediment,j)sample diluted due to high <br /> organic content <br /> DHS Certification No 1644 Angela Rydelius, Lab Manager <br />