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210 2nd Avenue South,#D7 Pacheco CA 94553-5560 <br /> McCampbell Analytical Inc Teiephone 925-798 1620 Fax 925-798-1622 <br />' <br /> http Hwww niccan7pbell corn F mail main mccampbell corn <br /> . Advanced GeoEnvironmental,Inc Client Project ID (Arco)Pacific Mini Date Sampled 02/25/03 <br /> 837 Shaw Road Mart Date Received 02/27/03 <br /> Client Contact Bill Little Date Extracted 03101103-03105103 <br /> Stockton,CA 95215 <br />' Client P O Date Analyzed 03101103-03105103 <br /> Oxygenates and BTEX by GC/MS* <br /> Extraction Method SW5030B Analytical Method SW8260B Work Order 0302377 <br /> Lab ID 0302377-005B 0302377-006B 0302377-007B 0302377-008B <br /> Client ID MW 5 MW 6 MW 7 MW 8 <br /> Reporting Limit for <br />' Matrix W W W I W --- DF=1 <br /> DF 20 1 ] 1 S W <br /> Compound Concentration ug/kg µg/L <br /> ten-Amyl methyl ether(TAME) ND<10 ND ND ND NA 05 <br />' Benzene 95 ND ND ND NA 05 <br /> t-Butyl alcohol(TBA) ND<100 19 ND ND NA 50 <br />' 1,2-Dibromoethane(EDB) ND<10 ND ND ND NA 05 <br /> 1,2-Dichloroethane(1,2-DCA) ND<10 ND ND ND NA 05 <br /> Dusopropyl ether(DIPS) ND<10 ND ND ND NA 0 5 <br /> lie <br /> Ethylbenzene 590 ND ND ND NA 0 5 <br /> Ethyl tent-butyl ether(LTBE) ND<10 ND ND ND NA 05 <br />' Methyl-t-butyl ether(MTBE) 460 11 ND 14 NA 0 5 <br /> Toluene ND<10 ND ND ND NA 05 <br /> Xylenes 82 ND ND ND — NA 0.3 <br /> Surrogate Recoveries (%) <br />' %SSI 111 118 122 119 <br />' %SS2 108 110 110 109 <br /> %SS3 923 947 95 1 950 <br /> Comments <br /> *water and vapor samples and all TCLP&SPLP extracts are reported in gg/L,soillsludge/solid samples to}ig/kg, wipe samples in liglwipe, <br /> productloillnon-aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysts <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—2 vol %sediment,i)sample diluted due to high <br /> 3rgame content <br /> • <br /> 1 <br /> DHS Certification No 1644 J- Angela Rydehus, Lab Manager <br />