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110 2nd Avenue South,#137,Pacheco CA 94553-5560 <br /> 4 1 McCampbell Analytical Inc Telephone 925-798-1620 Fax 925-798-1622 <br /> hup//www mccampbell com E mail imrmcarnpbell cam <br /> Advanced GeoEnvlronmental,Inc Client Project ID (Arco)Pacific Mm] Date Sampled 02/25/03 <br /> Mart <br /> 837 Shaw Road Date Received 02/27/03 <br /> Client Contact Bill Little Date Extracted 03/01/03-03/05103 <br /> Stockton,CA 95215 <br /> Client P O Date Analyzed 03/01/03-03105103 <br /> Oxygenates and BTEX by GC/MS* <br /> Extraction Method SW5030B Analytical Method SW8260B Work Order 0302377 <br /> Lab ID 0302377-00913 0302377-OIOB 0302377-01113 0302377-012B <br /> Client ID MW 9 MW 1O MW 1 IA MW 1113 <br /> Reporting Limit for <br />' Matnx �- W — ------W ----W-- -----W- ----- DF=! <br /> :D:FF1 1 20 5 S W <br /> I Compound Concentration ug/kg 11 <br /> 9l1- <br /> tert-Amyl methyl ether(TAME) ND I ND ND<10 ND<2 5 NA 05 <br /> Benzene ND ND ND<10 ND<2 5 NA 0 5 <br /> t-Butyl alcohol(TBA) ND ND ND<100 ND<25 NA 5 0 <br /> I 1,2-Dibromoethane(EDB) ND ND ND<10 ND<2 5 NA 0 5 <br /> 1,2-Dichloroethane(1 2-DCA) ND ND ND<10 ND<2 5 NA I 0 5 <br /> Dttsopropyl ether(RIPE) ND ND ND<10 ND<2 5 NA 0 5 <br /> 10 Ethylbenzene ND ND ND<10 ND<2 5 NA 0 5 <br /> Ethyl tert-butyl ether(ETBE) ND ND ND<10 ND<2 5 NA 0 5 <br />' Methyl-t-butyl ether(MTBE) ND ND 580 130 NA 05 <br /> Toluene ND ND ND<10 ND<2 5 NA 05 <br />' Xylenes NDND ND<10 ND<2 5 NA I 05 <br /> Surrogate Recoveries(%) <br />' %SS1 120 119 115 118 <br /> %SS2 110 111 102 107 <br />' %SS3 965 960 114 95 0 <br /> Comments t <br /> •water and vapor samples and all TCLP&SPLP extracts are reported to gg/L,soil/sludge/solid samples inµg/kg, wipe samples to Ag/wipe, <br /> product/oil/non-aqueous liquid samples to mg/L <br />' ND means not detected above the reporting limit,NIA means analyte not applicable to this analysts <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—2 vol %sediment,j)sample diluted due to high <br /> organic content <br /> 0 <br /> DHS Certification No 1644 JQ-Angela Rydehus, Lab Manager <br /> 1 <br />