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110 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> / mccam, beim E-mail main@mccampbell conn <br /> Date Sampled 06/15/98 <br /> Advanced GeoEnvironmental Ment Project M #0128,Arco <br /> 4005 North Wilson Way Date Received 06/17/98 <br /> Stockton,CA 95205 Client Contact B111 Little Date Extracted 06/19/98 <br /> Client P O Date Analyzed 06/19/98 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 90586 <br /> Client ID MW4/6-15-98 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> I Acetone" ND<15 Ethylbenzene 77 <br /> Benzene 45 Hexachlorobutadiene ND<S <br /> Bromobenzene ND<5 lodomethane ND<5 <br />] Bromochloromethane ND<5 Isopropylbenzene 56 <br /> Bromodichloromethane ND<5 p-Isopropyl toluene ND<5 <br /> Bromofonn ND<5 Methyl buryi ketoneND<5 <br /> Bromomethane ND<5 Methylene Chlondc"' ND<5 <br /> n-Butyl benzene ND<5 Methyl ethyl ketone... ND<5 <br /> sec-Butyl benzene ND<5 Methyl isobutyl ketone" ND<5 <br /> ten-Butyl benzene ND<5 Methyl tent-Butyl Ether(MTBE) <br /> Carbon Disulfide ND<5 Naphthalene ND<50 <br /> Carbon Tetrachlonde ND<5 n-Propyl benzene ND<5 <br /> Chlorobenzene ND<5 Styrene MND<5 <br /> Chloroethane ND<5 1,1,1,2-Tetrach1oroethane ND<5 <br /> 2-Chloroethyl Vinyl Ether ND<5 1,1,2,2-Tetrachloroethane NIKS <br /> Chloroform ND<5 Tetrachloroethene ND<5 <br /> Chloromethane ND<5 Toluene 29 <br /> 2-Chlorotoluene A'D<5 1,2,3-Tnchl orobenzene ND<5 <br /> 4-Chlorotoluene ND<5 1,2,4-Tnchlorobenzene ND<5 <br /> i Dibromochloromethane ND<5 1,1,1-Tnchloroethane ND<5 <br /> 1,2-Dibromo-3-chloropropane ND<5 1,42-Tnchloroethane ND<5 <br /> Dibromomethane ND<5 Trichloroethene ND<5 <br /> 1,2-Dichlorobenzene ND<5 Trichlorofluoromethane ND<5 <br /> I 1,3-Dichlorobenzene ND<5 1,2,3-Tnchloropropane ND<5 <br /> 1,4-Dichlorobenzene ND<5 1,2 4-Tnmethylbenzene 130 <br /> Dichlorodifluoromethane ND<5 1,3,5-Tnmethylbenzene 38 <br /> 1,1-Dichloroethane ND<5 Vinyl Acetate's ND<5 <br /> 12-Dlchloroethane ND<5 Vinyl Chloride" ND<5 <br /> l,1-Diehloroethene ND<5 Xylenes,total '° 140 <br /> cis-1,2-Dichloroethene ND<5 <br /> trans-1,2-Dichloroethene ND<5 <br /> 1,2-Dichloropropane ND<5 <br /> I J-Dichlorotiroaane ND<5 <br /> 2,2-Dichloropropane ND<5 Comments: <br /> 1,1-Dichloropropcne ND<5 Surrogate Recosenes(%) <br /> cis-1,3-Dachloropropene ND<5 Dibromofluoromethane 109 <br /> trans-l,3-Dichloropropene ND<5 Toluene-d8 103 <br /> Ethylene dibromideND<5 4-Bromofluorobenzene 98 <br /> -water and vapor samples are reported in ug/I-,soil and sludge samples in ug/kg,wipes in uglwtpe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 10 ug/l-, vapor samples 0.5 uSA, solid and sludge samples 5 ug/kg, wipes <br /> 0.2ug/wipe ND means not detected above the reporting lint,NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c)(2-chloroethoxy)ethene, (d) 2-hexanone, (e) dichloroniethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone,(h)lighter than water immiscible sheen is presenia (1)liquid sample that contains greater than—5 vol <br /> sediment,0)sample diluted due to high organic content,(k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte,p)methylbenzene,(m)acetic acid ethenyl ester,(n)chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br /> r <br />