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E <br /> l 10 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> htM-/Jwww_mecainy hdLr.= E-mail main@mccampbell eom <br /> Advanced Geo£nvironmentalDate Sampled 06/15/98 <br /> Client Protect XD ; 128,Arco <br /> Date Received 06/17/98 <br /> 4005 North Wilson Way <br /> Stockton, CA 95205 Client Contact Bill Little Date Extracted 06/19/98 <br /> Client P 0 Date Analyzed 06/19/98 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 90587 <br /> Client ID MW3/6-15-98 <br /> Matrix W <br /> Compound Concentration' Compound Concentration* <br /> Acetone" ND<2 Eihylbenzene ND <br /> Benzene ND Hcxachlorobutadiene ND <br /> Bromobenzene ND lodomethane ND <br /> Bromochloromethane ND Isopropylbenzene ND <br /> Bromodichloromethane ND p-Isopropyl toluene ND <br /> Bromoform ND Methyl butyl ketoneND <br /> Bromomethane ND Methylene Chloride"' ND <br /> n-Butyl benzene ND Methyl ethyl ketone ' ND <br /> sec-Butyl benzene ND Methyl isobutyl ketone u ND <br />` ten-Butyl benzene ND Methyl ten-Butyl Ether(MTBE) --- <br /> Carbon Disulfide ND Naphthalene ND<25 <br /> Carbon Tetrachloride ND n-Propyl benzene ND <br /> Chlorobenzene ND ST Nene MND <br /> Chloroethane ND 1,1,1,2-Tetrachloroethane ND <br /> 2-Chloroethyl Vinyl Ether" ND 1,1,2,2-Tetrachloroethane ND <br /> Chloroform ND Tetrachloroethene ND <br /> I Chloromethane tw°D Toluene ND <br /> 2-Chlorotoluene ND 1,2,3-Tnehlorobenzene ND <br /> 4- hlorotoluene ND 1,2,4-Tnchlorobenzene ND <br /> Dibromochloromethane ND 1,1,1-Tnchloroethane ND <br /> f 1,2-Dibromo-3-chlompropane ND 1,1,2-Trichloroethane ND <br />`i Dibromomethane ND Tnchloroethene ND <br /> 1,2-Dichlorobenzene ND Trichlorofluoromethane ND <br /> 1,3-Dichlorobenzene ND 1,2,3-Tnchloropropane ND <br /> I 1,4-Dichlorobenzene ND 1,2,4-Tnmethylbenzene ND <br /> Dichlorodifluoromethane ND 1,3,5-Tnmethylbenzene ND <br /> ],1-Dich10r0e1hane ND \inyl Acetate"I ND <br /> 1,2-Dichloroethane 24 Vinyl Chloride'"' ND <br /> I ],1-Dichloroethene ND X)lenes,total '° ND <br /> cis-1,2-Dichlorcethene ND <br /> trans-1,2-Dicbloroethene ND <br /> 1,2-Dichloropropane ND <br /> ],3-Dichloropropane ND <br /> 2,2-Dichloroprop2ne ND Comments <br /> ],1-Dichloropropene ND Surrogate Recoveries(%) <br /> cis-1,3-Dichloropropene ND Dibromofluoromethane 111 <br /> trans-1,3-Dichloropropene ND Toluen"S 144 <br /> Ethylene dibromide ND 4-Bromofluorobenzene 95 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP 1 SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 10 ug/L, vapor samples 0.5 ug/L, solid and sludge samples 5 ug/kg, wipes <br /> 0.2ug/wipe ND means not detected above the reporting hrrut,N/A means analyte not applicable to this analysis , <br /> (b) 2 propanone or dimethyl ketone, (c)(2-chloroethoxy)ethene, (d) 2-hcxanone, (e) dichloromethane, (f) 2-bmanone, (g) 4-rixthyl-2- <br /> pentanone or isopropylacetone, (h)lighter thari water immiscible sheen is present;(i)liquid sample that contains greater than —5 vol % <br /> sediment,0)sample diluted due to high organic content,(k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte,p)methylbenzene,(m)acetic acid ethenyl ester,(n)ch)oroethene,(o)dimethylbepzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br /> I <br />