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110 2nd Avenue South #D7 Pacheco CA 94553 5560 <br /> McCampbell Analytical, Inc. Telepboiie 925-798-1620 Fax 925-798-1622 <br /> 14 1 Website www iticcariipbcll coin E-mail train(a)imcanipbell cam <br /> Port of Stockton Client Project ID Port of Stockton UST Date Sampled 02/24/05 <br /> Site No 3 <br /> P O Box 2089 Date Received 03/10/05 <br /> Stockton CA 95201-20$9 Client Contact Rita Koehnen Date Extracted 03110/05-03/11/05 <br />' Client P O Date Analyzed 03/10/05-03/11105 <br /> BTEX by GC/MS* <br />' Extmcuan Method SW50108 Analytical Method SWB260B Work Order 0501118 <br /> Lab ID 0503178-OOIB 0503178-002B 0503178-003B 0503178-0048 <br /> Client ID MW3-1 MW3-2 MW3-3 MW3-4 <br /> Reporting Limit for <br /> Matrix W l W W W Df=I <br /> DF i - --— 10 -- 10 — 1 --- S w <br />' Compound Concentration uglkg pg/L <br /> Benzene ND I 71 NI)<5 0 ND NA 0 5 <br /> - - <br /> 1 � I <br /> 1=thylbenzene 1 1 � 65 I 28 I ND NA 0 5 <br /> Toluene 23 280 200 ND NA 0 5 <br /> I <br /> Xylenes 8 7 480 260 ND NA 0 5 <br /> v <br /> Surrogate Recoveries(%) <br /> %SS1 Ill 1 109 108 106 <br /> %SS2 102 100 103 _ 104 <br /> %SS3 86 --89 90 88 <br />' Commegis <br /> *water and vapar samples are reported toµg/L soil/sludge/solid samples in mg/kg pixrduct/oil/non aqueous liquid samples and all TC LP&SPLP <br /> extracts are reported in mg1L wipe samples in pg/wipe <br /> ND means not detected above the reporting limit NIA mans analyte not applicable to this analysts <br /> #surrogate diluted out of range or surrogate coelutes with another peak <br />' h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—1 vol %sediment j)sample diluted due to high <br /> organic c0ntent/m3tnx interference,k)reporting limn near,but not identical to our standard reporting limit due to variable FneOTL sample weight m) <br /> reeorting limit raised due to insufficient sample amount n results are reported on a d weight basis, )see attached narrative <br />' DHS Certification No 1644 Angela Rydelius,Lab Manager <br /> 1 <br />