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110 2nd Avenue South #D7 Pacheco C A 94553 5560 <br /> McCampbell Analytical, Inc. Telephone 925 798-1620 Fax 925 798 1622 <br /> 14 1 V ebstte www mccanipbell corn L-rnul matri(iotnecarnpbell corn <br /> Port of Stockton Client Project ID Port of Stockton UST Date Sampled 02/24/05 <br /> Site No 3 Date Received 03/10/05 <br /> P O Box 2059 <br /> Client Contact Rita Koehnen Date Extracted 03/10/05-03111/05 <br /> Stockton, CA 95201-2089 <br /> Client P O Date Analyzed 03110/05-03/11/05 <br />- - - - - - BTEX by GC/1VMS* <br /> Extraction Metlod Sw5030B Analytical Method SW826013 Work Order 050317a <br /> Lab 1D 0503178-0058 0503178-006B 0503178-0078 , <br /> Client 1D MW3-5 MW3-6 Trip Blank Reporting.Limit for <br /> MaEnx W W W — DF=I <br /> DF 1 SO 1 S W <br /> Compound Concentration ug/kg µg" ' <br /> Benzene ND 1200 ND i NA 0i <br /> Ethylbenzene ND NDc25 ND NA 0 5 <br /> Toluene ND ND<25 ND NA 05 <br /> Xylenes ND 54 ND NA 0 5 <br /> i <br /> Surrogate Recoveries(°/r►) <br /> ri6ssl los , los 107 <br /> %552 101 105 103 , <br /> %S43 87 89 89 <br /> Comments <br /> •water and vapor samples are reported to ptg/L sod/sludge/solid samples ming/kgpraduUtoillnon-dqueous liquid samples and all TO P&SPLP - <br /> extracts are reported in mg/L wtpe samples in pglwipc <br /> ND means not detected above the reporting limit NIA means analyte not applicable to this analysts ' <br /> #surrogate diluted out of range or surrogate coelutes with another peak <br /> h)lighter than wales immiscible sheen/product is present,i)liquid sample that contains greater than-1 vol %ssdtment,3)sample diluted due to high <br /> arga_mc content/matnx interference It7 reporting 11mti near but not identical to our standard reporting limit due to variable Encore sample weight nt) <br /> TrportiU limit raised due to insuffit-tent sample amount,it)results are±!-tied on a dry weight basis )see attached narrative <br /> DHS Certification No 1644 Angela Rydeltus,Lab Manager , <br /> 1 <br />