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110 2nd Avenue South MD? Pacheco CA 94553 5560 <br /> McCampbell Analytical, Inc. Telephone 925 798-1620 Fax 925 798 1622 <br /> Website www mccanipbcll com E-mail orampri-ccamili com <br /> QC SUMMARY REPORT FOR SW8021 B18015Cm <br />' W O Sample Matrix Water ac Matrix Water WorkOrder 0503178 <br /> EPA Method SW8021BI8015Cm Extraction SW5030B BatchlD 15301 Spiked Sample ID 0503168-001A <br />' Analyte Sample Splked 1i MSD' I MS-MSD' LCS LCSD LCS-LCSD Acceptance Criteria(%) <br /> ii pgIL %Rec %Rec %RPD %Rec %Rec % RPD MS 1 MSD LCS 1 LCSD <br />' TPH(btcx)r ND 60 95 965 1 55 95 8 92 1 382 70-130 70-t30 <br /> M rBE ND t0 963 104 793 101 946 647 70-110 70 130 <br /> Benzene ND 10 102 I 104 I 1 96 107 104 320 70- 110 70 130 <br /> Toluene ND _ 10 102_ - 1024 <br /> _0 101 978 2 86 70- 130 70 130 <br /> Ethylbenzene ND 10 101 102 0 914 103 998 277 70-130 70-130 <br /> Xylenes ND 30 90 90 0 907 66 3 490 70 t30 70-130 <br /> %SS 98 10 112 111 0 654 1 114 124 0 70- 130 70 130 <br /> All target compounds in the Method Blank of this extraction batch were ND less than the method RL.with the following exceptions <br /> NONE <br /> BATCH 15301 SUMMARY <br /> Sample ID Date Sampled Date Extracted Date Analyzed Sample ID Date Sampled Date Extracted Date Analyzed <br /> 010317R-003A <br /> 01 178-001A 2124101 3110/05 6 06 PM 3/10105 6 06 PM 0503178 002A 2/24105 3111105 3 05 AM 3/11105 3 05 AM 2/24/05 3/10/05 9 44 PM 3110/05 9 44 PM 0103178-004A 2/24105 3110105 1 23 PM 3110105 1 23 1'M <br /> 0503178 005A 2124105 1/10105 1 57 PM 3110105 1 57 PM 0503178 006A 2124105 3110105 10 17 PM 3/10!05 10 17 PM <br /> 0503173-007A 2124105 3110105 4 46 PM 3/10105 4 46 PM <br /> III <br /> MS=Matrix Spike,MSD=k1latros Spike Duplicate LC5=LaboratoryControl Sample LCSD=Laboratory Control Sample Duplicate,RPD=Relative Percent Deviation <br /> %Recovery=1001(MSSomple)I(Amount Spiked) RPD=100'(MS- MSD)I((MS+MSD)12) <br /> MS I MSD spike recoveries and I or%RPD may fall outside of laboratory acceptance critena due to one or more of the following reasons a)the sample is mhomogonous <br /> AND contains significant concenlrahcns of analyte relative to the amount spiked or b)the spiked sample s matrix interferes with the spike recovery <br /> E TPH(btex)=sum of 6TEX areas from the FID <br /> #cluttered chromatogram sample peak coelutes with surrogate peak <br /> NIA=not applicable or not enough sample to perform matrix spike and matrix spike duplicate <br /> =".1 e concentration in sampie exceeds spike amount for sod matnx or exceeds 2x spike amount for water matnx or sample diluted due to high matrix or analyte content <br /> IFIr <br />' � C Officer AI fi <br /> DHS Certification No 1644 � Q Q <br />