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Quality Control Results <br />Job Number: 720-1027-1Client: Kennedy/Jenks Consultants <br />Date Analyzed: <br />Date Analyzed: <br />Dilution: <br />Dilution: <br />12/22/2005 1347 <br />12/22/2005 1414 <br />Laboratory Control/ <br />Laboratory Control Duplicate Recovery Report - Batch: 720-3384 <br />1.0 <br />1.0 <br />Solid <br />LCS Lab Sample ID: <br />LCSD Lab Sample ID: <br />Client Matrix: <br />Date Prepared: <br />Units: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />Client Matrix:Solid <br />Date Prepared: <br />Units: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />mg/Kg <br />12/21/2005 1435 <br />Prep Batch: 720-3384 <br />Analysis Batch: 720-3483 <br />d:\data\200512\122205\LCS <br />30.05 g <br />1 mL <br />d:\data\200512\122205\LCSD <br />30.04 g <br />1 mL <br />mg/Kg <br />12/21/2005 1435 <br />Analysis Batch: 720-3483 <br />Prep Batch: 720-3384 <br />Method: 8270C <br />Preparation: 3550B <br />Sat 2K1 <br />Sat 2K1 <br />LCS 720-3384/2-A <br />LCSD 720-3384/3-A <br />Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS <br />% Rec. <br />7477 5 - 112 3 35Phenol <br />7880 12 - 158 2 35Bis(2-chloroethyl)ether <br />7473 23 - 134 1 352-Chlorophenol <br />7376 9 - 172 4 351,3-Dichlorobenzene <br />7371 20 - 124 2 351,4-Dichlorobenzene <br />7982 10 - 130 3 35Benzyl alcohol <br />7376 32 - 129 3 351,2-Dichlorobenzene <br />8077 10 - 130 3 352-Methylphenol <br />149152 10 - 130 2 35 **4-Methylphenol <br />7073 9 - 230 4 35N-Nitrosodi-n-propylamine <br />8078 40 - 113 3 35Hexachloroethane <br />8583 35 - 180 3 35Nitrobenzene <br />8386 21 - 196 4 35Isophorone <br />8584 29 - 182 0 352-Nitrophenol <br />7982 32 - 119 4 352,4-Dimethylphenol <br />8281 33 - 184 2 35Bis(2-chloroethoxy)methane <br />8280 10 - 130 2 352,4-Dichlorophenol <br />8382 44 - 142 1 351,2,4-Trichlorobenzene <br />8074 21 - 133 7 35Naphthalene <br />4042 10 - 130 5 354-Chloroaniline <br />8282 24 - 116 0 35Hexachlorobutadiene <br />8793 10 - 130 7 354-Chloro-3-methylphenol <br />8286 10 - 130 5 352-Methylnaphthalene <br />9181 10 - 130 12 35Hexachlorocyclopentadiene <br />7973 37 - 144 8 352,4,6-Trichlorophenol <br />8680 10 - 130 6 352,4,5-Trichlorophenol <br />9283 10 - 130 10 352-Chloronaphthalene <br />8488 10 - 130 4 352-Nitroaniline <br />9589 9 - 112 6 35Dimethyl phthalate <br />9284 33 - 145 9 35Acenaphthylene <br />8783 10 - 130 6 353-Nitroaniline <br />7975 47 - 145 6 35Acenaphthene <br />STL San Francisco <br />Calculations are performed before rounding to avoid round-off errors in calculated results. <br />Page 311 of 347