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Quality Control Results <br />Job Number: 720-1027-1Client: Kennedy/Jenks Consultants <br />Date Analyzed: <br />Date Analyzed: <br />Dilution: <br />Dilution: <br />12/22/2005 1347 <br />12/22/2005 1414 <br />Laboratory Control/ <br />Laboratory Control Duplicate Recovery Report - Batch: 720-3384 <br />1.0 <br />1.0 <br />Solid <br />LCS Lab Sample ID: <br />LCSD Lab Sample ID: <br />Client Matrix: <br />Date Prepared: <br />Units: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />Client Matrix:Solid <br />Date Prepared: <br />Units: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />mg/Kg <br />12/21/2005 1435 <br />Prep Batch: 720-3384 <br />Analysis Batch: 720-3483 <br />d:\data\200512\122205\LCS <br />30.05 g <br />1 mL <br />d:\data\200512\122205\LCSD <br />30.04 g <br />1 mL <br />mg/Kg <br />12/21/2005 1435 <br />Analysis Batch: 720-3483 <br />Prep Batch: 720-3384 <br />Method: 8270C <br />Preparation: 3550B <br />Sat 2K1 <br />Sat 2K1 <br />LCS 720-3384/2-A <br />LCSD 720-3384/3-A <br />Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS <br />% Rec. <br />9082 9 - 191 9 352,4-Dinitrophenol <br />8882 10 - 130 7 354-Nitrophenol <br />88 10 - 130 1 35 **Dibenzofuran <br />9085 39 - 139 6 352,4-Dinitrotoluene <br />10090 50 - 158 11 352,6-Dinitrotoluene <br />10396 9 - 114 7 35Diethyl phthalate <br />8787 25 - 158 0 354-Chlorophenyl phenyl ether <br />8987 59 - 121 3 35Fluorene <br />8887 10 - 130 2 354-Nitroaniline <br />8983 9 - 181 8 352-Methyl-4,6-dinitrophenol <br />9499 10 - 130 5 35N-Nitrosodiphenylamine <br />9996 53 - 127 3 354-Bromophenyl phenyl ether <br />9381 9 - 152 14 35Hexachlorobenzene <br />10289 14 - 176 14 35Pentachlorophenol <br />9496 10 - 130 2 35Phenanthrene <br />9090 27 - 133 1 35Anthracene <br />10193 10 - 130 8 35Di-n-butyl phthalate <br />9190 26 - 137 1 35Fluoranthene <br />116103 52 - 115 11 35 *Pyrene <br />10596 10 - 130 10 35Butyl benzyl phthalate <br />7370 10 - 130 5 353,3'-Dichlorobenzidine <br />10388 33 - 143 15 35Benzo[a]anthracene <br />9987 8 - 158 13 35Bis(2-ethylhexyl) phthalate <br />10693 17 - 168 13 35Chrysene <br />10091 4 - 146 10 35Di-n-octyl phthalate <br />9493 24 - 159 1 35Benzo[b]fluoranthene <br />9498 17 - 163 4 35Benzo[a]pyrene <br />8394 11 - 162 12 35Benzo[k]fluoranthene <br />97102 9 - 171 5 35Indeno[1,2,3-cd]pyrene <br />10397 9 - 219 7 35Benzo[g,h,i]perylene <br />3842 10 - 130 9 35Benzoic acid <br />8780 10 - 130 9 35Azobenzene <br />STL San Francisco <br />Calculations are performed before rounding to avoid round-off errors in calculated results. <br />Page 312 of 347