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Quality Control Results <br />Job Number: 720-1027-1Client: Kennedy/Jenks Consultants <br />Date Analyzed: <br />Date Analyzed: <br />Dilution: <br />Dilution: <br />12/22/2005 2312 <br />12/22/2005 2341 <br />Solid <br />Matrix Spike/ <br />Matrix Spike Duplicate Recovery Report - Batch: 720-3384 <br />10 <br />10 <br />MS Lab Sample ID: <br />MSD Lab Sample ID: <br />Client Matrix: <br />Date Prepared: <br />Date Prepared: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />Client Matrix:Solid <br />Analysis Batch: 720-3483 <br />Analysis Batch: 720-3483 <br />12/21/2005 1435 <br />12/21/2005 1435 <br />Prep Batch: 720-3384 <br />Prep Batch: 720-3384 <br />d:\data\200512\122205\720-1 <br />30.10 g <br />5 mL <br />d:\data\200512\122205\720-10 <br />30.08 g <br />5 mL <br />Method: 8270C <br />Preparation: 3550B <br />Sat 2K1 <br />Sat 2K1 <br />720-1027-34 <br />720-1027-34 <br />Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS <br />% Rec. <br />91 69 17 - 163 27 35Benzo[a]pyrene <br />83 60 11 - 162 31 35Benzo[k]fluoranthene <br />40 100 9 - 171 NC 35Indeno[1,2,3-cd]pyrene <br />50 124 9 - 219 85 35 *Benzo[g,h,i]perylene <br />8 10 10 - 130 NC 35 *Benzoic acid <br />68 77 10 - 130 11 35Azobenzene <br />44 45 10 - 130 NC 35Dibenz(a,h)anthracene <br />Surrogate MS % Rec MSD % Rec Acceptance Limits <br />Nitrobenzene-d5 52 32 23 - 120 <br />2-Fluorobiphenyl 88 102 30 - 115 <br />Terphenyl-d14 66 0 18 - 137* <br />2-Fluorophenol 43 36 25 - 121 <br />Phenol-d5 39 34 24 - 113 <br />2,4,6-Tribromophenol 85 78 19 - 122 <br />STL San Francisco <br />Calculations are performed before rounding to avoid round-off errors in calculated results. <br />Page 316 of 347