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Quality Control Results <br />Job Number: 720-1027-1Client: Kennedy/Jenks Consultants <br />Date Analyzed: <br />Date Analyzed: <br />Dilution: <br />Dilution: <br />12/22/2005 2312 <br />12/22/2005 2341 <br />Solid <br />Matrix Spike/ <br />Matrix Spike Duplicate Recovery Report - Batch: 720-3384 <br />10 <br />10 <br />MS Lab Sample ID: <br />MSD Lab Sample ID: <br />Client Matrix: <br />Date Prepared: <br />Date Prepared: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />Client Matrix:Solid <br />Analysis Batch: 720-3483 <br />Analysis Batch: 720-3483 <br />12/21/2005 1435 <br />12/21/2005 1435 <br />Prep Batch: 720-3384 <br />Prep Batch: 720-3384 <br />d:\data\200512\122205\720-1 <br />30.10 g <br />5 mL <br />d:\data\200512\122205\720-10 <br />30.08 g <br />5 mL <br />Method: 8270C <br />Preparation: 3550B <br />Sat 2K1 <br />Sat 2K1 <br />720-1027-34 <br />720-1027-34 <br />Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS <br />% Rec. <br />80 81 33 - 145 NC 35Acenaphthylene <br />62 53 10 - 130 15 353-Nitroaniline <br />66 75 47 - 145 13 35Acenaphthene <br />0 0 9 - 191 NC 35 **2,4-Dinitrophenol <br />83 88 10 - 130 5 354-Nitrophenol <br />75 78 10 - 130 4 35Dibenzofuran <br />43 45 39 - 139 5 352,4-Dinitrotoluene <br />76 60 50 - 158 23 352,6-Dinitrotoluene <br />89 90 9 - 114 1 35Diethyl phthalate <br />83 84 25 - 158 1 354-Chlorophenyl phenyl ether <br />84 75 59 - 121 12 35Fluorene <br />70 62 10 - 130 NC 354-Nitroaniline <br />0 3 9 - 181 NC 35 **2-Methyl-4,6-dinitrophenol <br />81 77 10 - 130 5 35N-Nitrosodiphenylamine <br />45 48 53 - 127 NC 35 **4-Bromophenyl phenyl ether <br />93 84 9 - 152 10 35Hexachlorobenzene <br />39 42 14 - 176 NC 35Pentachlorophenol <br />85 75 10 - 130 13 35Phenanthrene <br />75 63 27 - 133 16 35Anthracene <br />83 78 10 - 130 6 35Di-n-butyl phthalate <br />72 65 26 - 137 11 35Fluoranthene <br />93 98 52 - 115 5 35Pyrene <br />79 90 10 - 130 NC 35Butyl benzyl phthalate <br />36 36 10 - 130 NC 353,3'-Dichlorobenzidine <br />80 51 33 - 143 44 35 *Benzo[a]anthracene <br />86 82 8 - 158 5 35Bis(2-ethylhexyl) phthalate <br />88 88 17 - 168 NC 35Chrysene <br />77 99 4 - 146 25 35Di-n-octyl phthalate <br />84 87 24 - 159 4 35Benzo[b]fluoranthene <br />STL San Francisco <br />Calculations are performed before rounding to avoid round-off errors in calculated results. <br />Page 315 of 347