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Quality Control Results <br />Job Number: 720-1027-1Client: Kennedy/Jenks Consultants <br />Date Analyzed: <br />Date Analyzed: <br />Dilution: <br />Dilution: <br />12/26/2005 1249 <br />12/26/2005 1316 <br />Solid <br />Matrix Spike/ <br />Matrix Spike Duplicate Recovery Report - Batch: 720-3494 <br />1.0 <br />1.0 <br />MS Lab Sample ID: <br />MSD Lab Sample ID: <br />Client Matrix: <br />Date Prepared: <br />Date Prepared: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />Client Matrix:Solid <br />Analysis Batch: 720-3536 <br />Analysis Batch: 720-3536 <br />12/23/2005 1159 <br />12/23/2005 1159 <br />Prep Batch: 720-3494 <br />Prep Batch: 720-3494 <br />d:\data\200512\122605\720-1 <br />30.11 g <br />1 mL <br />d:\data\200512\122605\720-10 <br />30.15 g <br />1 mL <br />Method: 8270C <br />Preparation: 3550B <br />Sat 2K1 <br />Sat 2K1 <br />720-1035-A-49-B MS <br />720-1035-A-49-C MSD <br />Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS <br />% Rec. <br />80 81 5 - 112 0 35Phenol <br />81 78 12 - 158 4 35Bis(2-chloroethyl)ether <br />79 75 23 - 134 6 352-Chlorophenol <br />73 71 9 - 172 3 351,3-Dichlorobenzene <br />68 70 20 - 124 2 351,4-Dichlorobenzene <br />87 79 10 - 130 10 35Benzyl alcohol <br />73 73 32 - 129 1 351,2-Dichlorobenzene <br />80 80 10 - 130 1 352-Methylphenol <br />161 156 10 - 130 3 35 **4-Methylphenol <br />73 71 9 - 230 3 35N-Nitrosodi-n-propylamine <br />75 73 40 - 113 2 35Hexachloroethane <br />93 87 35 - 180 6 35Nitrobenzene <br />92 85 21 - 196 8 35Isophorone <br />92 88 29 - 182 4 352-Nitrophenol <br />90 83 32 - 119 8 352,4-Dimethylphenol <br />91 83 33 - 184 9 35Bis(2-chloroethoxy)methane <br />92 84 10 - 130 9 352,4-Dichlorophenol <br />84 79 44 - 142 6 351,2,4-Trichlorobenzene <br />81 71 21 - 133 14 35Naphthalene <br />56 53 10 - 130 4 354-Chloroaniline <br />76 74 24 - 116 3 35Hexachlorobutadiene <br />101 93 10 - 130 8 354-Chloro-3-methylphenol <br />89 78 10 - 130 13 352-Methylnaphthalene <br />77 77 10 - 130 0 35Hexachlorocyclopentadiene <br />87 83 37 - 144 6 352,4,6-Trichlorophenol <br />94 92 10 - 130 3 352,4,5-Trichlorophenol <br />87 82 10 - 130 6 352-Chloronaphthalene <br />90 85 10 - 130 6 352-Nitroaniline <br />97 91 9 - 112 7 35Dimethyl phthalate <br />STL San Francisco <br />Calculations are performed before rounding to avoid round-off errors in calculated results. <br />Page 322 of 347