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Quality Control Results <br />Job Number: 720-1027-1Client: Kennedy/Jenks Consultants <br />Date Analyzed: <br />Date Analyzed: <br />Dilution: <br />Dilution: <br />12/26/2005 1249 <br />12/26/2005 1316 <br />Solid <br />Matrix Spike/ <br />Matrix Spike Duplicate Recovery Report - Batch: 720-3494 <br />1.0 <br />1.0 <br />MS Lab Sample ID: <br />MSD Lab Sample ID: <br />Client Matrix: <br />Date Prepared: <br />Date Prepared: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />Client Matrix:Solid <br />Analysis Batch: 720-3536 <br />Analysis Batch: 720-3536 <br />12/23/2005 1159 <br />12/23/2005 1159 <br />Prep Batch: 720-3494 <br />Prep Batch: 720-3494 <br />d:\data\200512\122605\720-1 <br />30.11 g <br />1 mL <br />d:\data\200512\122605\720-10 <br />30.15 g <br />1 mL <br />Method: 8270C <br />Preparation: 3550B <br />Sat 2K1 <br />Sat 2K1 <br />720-1035-A-49-B MS <br />720-1035-A-49-C MSD <br />Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS <br />% Rec. <br />84 87 33 - 145 3 35Acenaphthylene <br />89 91 10 - 130 2 353-Nitroaniline <br />79 83 47 - 145 4 35Acenaphthene <br />72 83 9 - 191 14 352,4-Dinitrophenol <br />85 81 10 - 130 5 354-Nitrophenol <br />1 7 10 - 130 141 35 **Dibenzofuran <br />93 89 39 - 139 5 352,4-Dinitrotoluene <br />98 93 50 - 158 5 352,6-Dinitrotoluene <br />94 95 9 - 114 2 35Diethyl phthalate <br />91 88 25 - 158 4 354-Chlorophenyl phenyl ether <br />87 78 59 - 121 10 35Fluorene <br />100 97 10 - 130 3 354-Nitroaniline <br />92 86 9 - 181 7 352-Methyl-4,6-dinitrophenol <br />95 90 10 - 130 6 35N-Nitrosodiphenylamine <br />88 83 53 - 127 6 354-Bromophenyl phenyl ether <br />88 76 9 - 152 15 35Hexachlorobenzene <br />97 96 14 - 176 1 35Pentachlorophenol <br />90 84 10 - 130 8 35Phenanthrene <br />83 88 27 - 133 5 35Anthracene <br />88 87 10 - 130 1 35Di-n-butyl phthalate <br />81 78 26 - 137 3 35Fluoranthene <br />94 93 52 - 115 0 35Pyrene <br />84 89 10 - 130 5 35Butyl benzyl phthalate <br />66 71 10 - 130 8 353,3'-Dichlorobenzidine <br />78 81 33 - 143 4 35Benzo[a]anthracene <br />83 84 8 - 158 1 35Bis(2-ethylhexyl) phthalate <br />89 87 17 - 168 2 35Chrysene <br />83 84 4 - 146 1 35Di-n-octyl phthalate <br />77 83 24 - 159 8 35Benzo[b]fluoranthene <br />STL San Francisco <br />Calculations are performed before rounding to avoid round-off errors in calculated results. <br />Page 323 of 347