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Quality Control Results <br />Job Number: 720-1027-1Client: Kennedy/Jenks Consultants <br />Date Analyzed: <br />Date Analyzed: <br />Dilution: <br />Dilution: <br />12/26/2005 1249 <br />12/26/2005 1316 <br />Solid <br />Matrix Spike/ <br />Matrix Spike Duplicate Recovery Report - Batch: 720-3494 <br />1.0 <br />1.0 <br />MS Lab Sample ID: <br />MSD Lab Sample ID: <br />Client Matrix: <br />Date Prepared: <br />Date Prepared: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />Client Matrix:Solid <br />Analysis Batch: 720-3536 <br />Analysis Batch: 720-3536 <br />12/23/2005 1159 <br />12/23/2005 1159 <br />Prep Batch: 720-3494 <br />Prep Batch: 720-3494 <br />d:\data\200512\122605\720-1 <br />30.11 g <br />1 mL <br />d:\data\200512\122605\720-10 <br />30.15 g <br />1 mL <br />Method: 8270C <br />Preparation: 3550B <br />Sat 2K1 <br />Sat 2K1 <br />720-1035-A-49-B MS <br />720-1035-A-49-C MSD <br />Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS <br />% Rec. <br />81 82 17 - 163 1 35Benzo[a]pyrene <br />76 77 11 - 162 2 35Benzo[k]fluoranthene <br />80 84 9 - 171 5 35Indeno[1,2,3-cd]pyrene <br />83 86 9 - 219 3 35Benzo[g,h,i]perylene <br />18 33 10 - 130 61 35 *Benzoic acid <br />83 77 10 - 130 7 35Azobenzene <br />82 88 10 - 130 8 35Dibenz(a,h)anthracene <br />Surrogate MS % Rec MSD % Rec Acceptance Limits <br />Nitrobenzene-d5 83 78 23 - 120 <br />2-Fluorobiphenyl 70 73 30 - 115 <br />Terphenyl-d14 71 78 18 - 137 <br />2-Fluorophenol 66 69 25 - 121 <br />Phenol-d5 74 74 24 - 113 <br />2,4,6-Tribromophenol 83 81 19 - 122 <br />STL San Francisco <br />Calculations are performed before rounding to avoid round-off errors in calculated results. <br />Page 324 of 347