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APEX ENVIROTECH, INC. STANDARD OPERATING PROCEDURE onitonfl+�Welis SOP - a SOP ` _ SAMPLE IDENTIFICATION AND CHAIN- SOIL BORING SAMPLING. OF-CUSTODY PROCEDURES During drilling,soil samples for chemical analysts are collected Sample identification and chain-of-custody procedures ensure in thin-walled brass tubes,of varying diameters and lengths sample integrity as well as document sample possession from (e g ,4 or 6 inches long by 2 inches outside diameter) Three the time of collection to ultimate disposal Each sample or four of the selected tubes,plus a spacer tube,are set in an container submitted for analysts is labeled to identify the lob 18-Inch long split-barrel sampler of the appropriate inside- number,date time of sample collection a sample number diameter unique to the sample any in-field measurements made, sampling methodology name(s)of on-site personnel,and any Where possible,the split-barrel sampler is do en its entire other pertinent field observations also recorded on the field length either hydraulically or using a 140-pound drop hammer excavation or boring log The sampler is extracted from the borehole and the brass tubes,containing the sod samples,are removed Upon removal Chain-of-custody forms are used to record possession of the from the sampler,the selected brass tubes are either sample from time of collection to arrival at the laboratory immediately trimmed and capped with aluminum foil or"Teflon" During shipment the person with custody of the samples will sheets and plastic caps or the samples are extruded from the relinquish them to the next person by signing the chain-of- tubes and seated within other appropriate,cleaned sample custody form(s)and noting the date and time The sample- containers The samples are then hermetically sealed,labeled, control officer at the laboratory wIli verify sample integrity, and refrigerated for delivery,under strict chain-of-custody,to correct preservation,confirm collection in the proper the analytical laboratory These procedures minimize the container(s),and ensure adequate volume for analysis potential for cross-contamination and volatilization of volatile organic compounds(VOC)prior to chemical analysts If these conditions are met the samples will be assigned unique laboratory log numbers for identification throughout One soil sample collected at each sampling interval is analyzed analysis and reporting The log numbers will be recorded on In the field using either a portable photoionization detector the chain-of-custody forms and in the legally-required tog book (PID),flame ionization detector organic vapor analyzer, maintained in the laboratory The sample description,date catalytic gas detector,or an explosimeter The purpose of this received clients name and any other relevant information will field analysis is to qualitatively determine the presence or also be recorded • absence of hydrocarbons and the samples to be analyzed at the laboratory The sod sample is sealed in either a brass tube, glass lar,or plastic bag to allow for some volatilization of VOC SOP _ 5 The PID is then used to measure the concentrations of LABORATORY ANALYTICAL QUALITY hydrocarbons within the containers's headspace The data is ASSURANCE AND CONTROL recorded on both field notes and the boning logs at the depth corresponding to the sampling point In addition to routine instrument calibration replicates spikes blanks,spiked blanks and certified reference materials are Other soil samples are collected to document the sod and/or routinely analyzed at method-specific frequencies to monitor stratigraphic profile beneath the project site,and estimate the precision and bias Additional components of the laboratory relative permeability of the subsurface materials All drilling Quality Assurancelouslity Control program include and sampling equipment are either steam cleaned or washed in solution and doubly rinsed in deiomzed water prior to use at 1 Participation in state and federal laboratory each site and between boreholes to minimize the potential for accreditation/certification programs, cross-contamination 2 Participation in both U S EPA Performance In the event the soil samples cannot be submitted to the Evaluation studies(WS and WP studies)and inter- analytical laboratory on the same day they are collected(e g, laboratory performance evaluation programs due to weekends or holidays),the samples are temporanly stored until the first opportunity for submittal either on ice in a 3 Standard operating procedures describing routine cooler such as when in the field,or in a refrigerator at Apexes and periodic instrument maintenance, office 4 "Out-of-Control"ICorrectnre Action documentation SOP - 3 procedures,and, SOIL CLASSIFICATION 5 Mufti-level review of raw data and client reports Soil samples are classified according to the Unified Sod Classification System Representative portions of the samples SOP . g may be submitted under strict chain-of-custody,to an HOLLOW—STEM AUGER MONITORING analytical laboratory for further examination and verification of WELL INSTALLATION AND the in-field classification and analysis of sod mechanical and/or DEVELOPMENT petrophysical properties The soil types are indicated on logs of either ex cavabons or borings together with depths Boreholes for monitoring wells are drilled using a truck- corresponding to the sampling points and other pertinent mounted,hollow-stem auger dnli ng The borehole diameter information will be a minimum of 4 inches larger than the outside diameter of the casing when installing well screen The hollow-stem auger provides minimal interruption of drilling while permitting