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819 Striker Avenue, Suite 8 <br /> Sequoia Sacramento, 95834 <br /> (916) 92 1-96009600 <br /> FAX(916)921-0100 <br /> Analyticalwww.sequoialabs.com <br /> Kleinfelder-Stockton Project: Mel Rice Terminal S405100 <br /> 2825 East Myrtle Street. Project Number: 43851.E01 Reported: <br /> Stockton CA,95205 Project Manager: Doug Heard 05/25/04 16:45 <br /> Conventional Chemistry Parameters by APHA/EPA Methods - Quality Control <br /> Sequoia Analytical- Sacramento <br /> Reporting Spike Source %REC RPU <br /> Analyte Result Limit Units Level Result %REC Limits RPD I_imic \oic <br /> Batch 4050309-General Preparation <br /> Matrix Spike(4050309-MSI) Source:S405120-03 Prepared&Analyzed:05/24/04 <br /> Ammonia as N 78.6 0.082 mg/l 82.2 1:9 93 75-125 <br /> Matrix Spike Dup(4050309-MSD1) Source:S405120-03 Prepared&Analyzed:05/24/04 <br /> Ammonia as N 81.4 0.082 mg/l 82.2 1.9 97 75-125 4 20 <br /> Sequoia Analytical-Sacramento The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document. Unless otherwise stated,results are reported on a wet weight basis. <br /> This analytical report must be reproduced in its entirety. <br /> Page 19 of 23 <br />