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819 Striker Avenue,Suite 8 <br /> Sequoia Sacramento,CA 95834 <br /> (916) 921-9600 <br /> FAX(916)92 1-0100 <br /> J%F Analytical www.sequoialabs.com <br /> Kleinfelder-Stockton Project: Mel Rice Terminal S405100 <br /> 2825 East Myrtle Street.. Project Number: 43851.E01 Reported: <br /> Stockton CA,95205 Project Manager: Doug Heard 05/25/04 16:45 <br /> Anions by EPA Method 300.0- Quality Control <br /> Sequoia Analytical- Sacramento <br /> Reporting Spike Source %REC RPD <br /> lnalyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch 4050093 -General Preparation <br /> Blank(4050093-BLKI) Prepared&Analyzed:05/05/04 <br /> Nitrate as N ND 0.023 mg/I <br /> Laboratory Control Sample(4050093-BS1) Prepared&Analyzed:05/05/04 <br /> Nitrate as N 1.18 0.023 mg/l 1.13 104 80-120 <br /> Laboratory Control Sample Dup(4050093-13SD1) Prepared&Analyzed:05/05/04 <br /> Nitrate as N 1.15 0.023 mg/I 1.13 102 80-120 3 20 <br /> Matrix Spike(4050093-MSI) Source:S404436-01 Prepared&Analyzed:05/05/04 <br /> Nitrate as N 12.9 0.23 mg/l 11.3 0.94 106 75-125 <br /> Matrix Spike(4050093-MS2) Source:S404479-01 Prepared&Analyzed:05/05/04 <br /> Nitrate as N 10000000000 0.23 mg/l 11.3 3.1 NR 75-125 QCOI <br /> Batch 4050144-General Prep <br /> Blank(4050144-BLKI) Prepared&Analyzed:05/07/04 <br /> Nitrate as N ND 0.023 mg/I <br /> Laboratory Control Sample(4050144-BS1) Prepared&Analyzed:05/07/04 <br /> Nitrate as N 1.13 0.023 mg/I 1.13 100 80-120 <br /> Laboratory Control Sample Dup(4050144-BSD1) Prepared&Analyzed:05/07/04 <br /> Nitrate as N 1.12 0.023 mg/l 1.13 99 80-120 0.9 20 <br /> Matrix Spike(4050144-MSI) Source:S405153-03 Prepared&Analyzed:05/07/04 <br /> Nitrate as N 16.7 0.23 mg/I 11.3 5.2 102 75-125 <br /> Sequoia Analytical-Sacramento The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document. Unless otherwise stated,results are reported on a wet weight basis. <br /> This analytical report must be reproduced in its entirety. <br /> Page 20 of 23 <br />