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819 Striker Avenue,Suite 8 <br /> Sequoia Sacramento, 92 95834 <br /> P140 <br /> c (916) 921-9600 <br /> FAX(916)921-0100 <br /> Analytical www.sequoialabs.com <br /> Kleinfelder-Stockton Project: Mel Rice Terminal S405100 <br /> 2825 East Myrtle Street., Project Number: 43851.E01 Reported: <br /> Stockton CA,95205 Project Manager: Doug Heard 05/25/04 16:45 <br /> Anions by EPA Method 300.0 - Quality Control <br /> Sequoia Analytical- Sacramento <br /> Reporting Spike Source %REC RPD <br /> Analyte Result I.in,it Units Level Result %REC Limits RPD Limit Notes <br /> Batch 4050268-General Preparation <br /> Matrix Spike(4050268-MSI) Source:S405100-10 Prepared&Analyzed:05/06/04 <br /> Nitrate as N 448 2.3 mg/kg 11.3 430 159 75-125 QCO1 <br /> Matrix Spike(4050268-MS2) Source:S405100-01 Prepared&Analyzed:05/06/04 <br /> Nitrate as N 12.9 2.3 mg/kg 11.3 1.3 103 75-125 <br /> Batch 4050269-General Preparation <br /> Blank(4050269-BLKI) Prepared&Analyzed:05/06/04 <br /> Nitrate as N ND 0.23 mg/kg <br /> Laboratory Control Sample(4050269-BS1) Prepared&Analyzed:05/06/04 <br /> Nitrate as N 11.5 0.23 mg/kg 11.3 102 80-120 <br /> Laboratory Control Sample Dup(4050269-BSDI) Prepared&Analyzed:05/06/04 <br /> Nitrate as N 11.6 0.23 mg/kg 11.3 103 80-120 0.9 200 <br /> Matrix Spike(4050269-MS1) Source:S405093-01 Prepared&Analyzed:05/06/04 <br /> Nitrate as N 11.1 2.3 mg/kg 11.3 ND 98 75-125 <br /> Sequoia Analytical - Sacramento The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document. Unless otherwise stated,results are reported on a wet weight basis. <br /> This analytical report must be reproduced in its entirety. <br /> Page 22 of 23 <br />