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819 Striker Avenue, Suite 8 <br /> Sequoia Sacramento, 92 95834 <br /> (916)921-9600 <br /> FAX(916)92 1-0100 <br /> 14C,!DO Analytical www.sequoialabs.com <br /> Kleinfelder-Stockton Project: Mel Rice Terminal 5405100 <br /> 2825 East Myrtle Street.. Project Number: 43851.E01 Reported: <br /> Stockton CA,95205 Project Manager: Doug Heard 05/25/04 16:45 <br /> Anions by EPA Method 300.0-Quality Control <br /> Sequoia Analytical- Sacramento <br /> Reporting Spike Source %REC RPD <br /> Analyte RcSolt Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch 4050144-General Prep <br /> Matrix Spike(4050144-MS2) Source:S405175-01 Prepared&Analyzed:05/07/04 <br /> Nitrate as N 12.8 0.23 mg/I 11.3 0.99 105 75-125 <br /> Batch 4050205-General Prep <br /> Blank(4050205-BLKI) Prepared&Analyzed:05/12/04 <br /> Nitrate as N ND 0.023 mg/l <br /> Laboratory Control Sample(4050205-BS1) Prepared&Analyzed:05/12/04 <br /> Nitrate as N 1.14 0.023 mg/l 1.13 101 80-120 <br /> Laboratory Control Sample Dup(4050205-BSD1) Prepared&Analyzed:05/12/04 <br /> Nitrate as N 1.14 0.023 mg/l 1.13 101 80-120 0 20 <br /> Matrix Spike(4050205-MSI) Source:5404562-01 Prepared&Analyzed:05/12/04 <br /> Nitrate as N 20.3 0.23 mg/l 11.3 8.9 101 75-125 <br /> Batch 4050268-General Preparation <br /> Blank(4050268-BLKI) Prepared&Analyzed:05/06/04 <br /> Nitrate as N ND 0.23 mg/kg <br /> Laboratory Control Sample(4050268-BSI) Prepared&Analyzed:05/06/04 <br /> Nitrate as N 11.7 0.23 mg/kg 11.3 104 80-120 <br /> Laboratory Control Sample Dup(4050268-BSD1) Prepared&Analyzed:05/06/04 <br /> Nitrate as N 11.8 0.23 mg/kg 11.3 104 80-120 0.9 200 <br /> Sequoia Analytical- Sacramento The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document.Unless otherwise stated,results are reported on a wet weight basis. <br /> This analytical report must be reproduced in its entirety. <br /> Page 21 of 23 <br />