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COLUMBIA ANALYTICAL SERVICES,INC <br /> Analytical Results <br /> Client Applied Earth Sciences, Incorporated Service Request X0400795 <br /> Project Canteen Corp/AGE-NC-99-0612 Date Collected 08/16/2004 <br /> pie Matrix Water Date Received 08/17/2004 <br /> Volatile Organic Compounds <br />' Sample Name MW-3/081604 Units ug/L <br /> Lab Code X0400795-001 Basis NA <br /> Extraction Method EPA 5030B Level Low <br />' Analysis Method 8260B <br /> Dilution Date Date Extraction <br /> IAnalyte Name Result Q MRL MDL Factor Extracted Analyzed Lot Note <br /> Methyl tort-Butyl Ether 100 D 10 80 10 09/13/04 09/13/04 XWG0400980 <br /> Benzene ND U 050 030 1 08/30/04 08/30/04 XWCT0400953 <br /> 1,2-Dichloroethane ND U 050 0 50 1 08/30/04 08/30/04 XWG0400953 <br /> Toluene ND U 050 020 1 08/30/04 08/30/04 XWG0400953 <br /> 1,2-Dibromoethane ND U 050 030 1 08/30/04 08/30/04 XWG0400953 <br /> Ethylbenzene ND U 050 020 1 08/30/04 08/30/04 XWG0400953 <br /> m,p-Xylenes ND U 10 060 1 08/30/04 08/30/04 XWG0400953 <br /> o-Xylene ND U 050 030 1 08/30/04 08/30/04 XWCT0400953 <br /> tert-Butyl Alcohol ND U 20 10 1 08/30/04 08/30/04 XWG0400953 <br /> Dnsopropyl Ether ND U 10 040 1 08/30/04 08/30/04 XWG0400953 <br /> tert-Amyl Methyl Ether ND U 0 50 030 1 08/30/04 08/30/04 XWG0400953 <br /> tert-Butyl Ethyl Ether ND U 050 030 1 08/30/04 08/30/04 XWG0400953 <br /> We Case Narrative <br /> Control Dafe <br /> Surrogate Naive %Rec Limas Analyzed Note <br /> Dibromofluoromethane 91 77-121 08/30/04 Acceptable <br /> Toluene-d8 88 65-131 08/30/04 Acceptable <br /> 4-Bromofluorobenzene 79 68-125 08/30/04 Acceptable <br /> I <br /> �ents <br /> Printed 09/20/2004 11 5105 Form 1A-Organic Page I of 1 <br /> L 1STEALTMCRYSTAL RPTIFormlm rpt Merged SuperSet Roference RR4937 <br />