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COLUMBIA ANALYTICAL SERVICES,INC <br /> Analytical Results <br /> Client Applied Earth Sciences, Incorporated Service Request. X0400795 <br /> Project Canteen Corp/AGE-NC-99-0612 Date Collected 08/16/2004 <br /> mple Matrix Water Date Received 08/17/2004 <br /> Volatile Organic Compounds <br /> Sample Naive MW-3A/081604 Units ug/1- <br /> Lab <br /> g/LLab Code X0400795-002 Basis NA <br /> Extraction Method EPA 5030B Level Low <br /> IAnalysis Method 8260E <br /> Dilution Date Date Extraction <br /> Analyte Name Result Q MRL MDL Factor Extracted Analyzed Lot Note <br /> Methyl tert-Butyl Ether 160 D 10 80 10 09/13/04 09/13/04 XWG0400980 <br /> Benzene ND U 050 030 1 08/30/04 08/30/04 XWG0400953 <br /> 1,2-D,,chloroethane ND U 0 50 0 50 1 08/30/04 08/30/04 XWG0400953 <br /> Toluene ND U 0 50 020 1 08/30/04 08/30/04 XWG0400953 <br /> 1,2-Dibromoethane ND U 050 030 1 08/30/04 08/30/04 XWG0400953 <br /> Ethylbenzene ND U 050 020 1 08/30/04 08/30/04 XWG0400953 <br /> Im,p-Xylenes ND U 10 060 1 08/30/04 08/30/04 XWG0400953 <br /> o-Xylene ND U 050 030 1 08/30/04 08/30/04 XWG0400953 <br /> tert-Butyl Alcohol ND U 20 10 1 08/30/04 08/30/04 XWG0400953 <br /> Diisopropyl Ether ND U 10 040 1 08/30/04 08/30/04 XWG0400953 <br /> tert-Amyl Methyl Ether ND U 050 030 1 08/30/04 08/30/04 XWG0400953 <br /> tert-Butyl Ethyl Ether ND U 050 030 1 08/30/04 08/30/04 XWG0400953 <br /> Isee Case Narrative <br /> Control Date <br /> Surrogate Name %Rec Limits Analyzed Note <br /> Dibromofluoromethane 103 77-121 08/30/04 Acceptable <br /> Toluene-d8 102 65-131 08/30/04 Acceptable <br /> 4-Bromofliuorobenzene 91 68-125 08/30/04 Acceptable <br /> O—ents <br />■ Printed 09/20/2004 11 51 08 Form I-Organic Page 1 of I <br /> i.1STHALTMCRYSTALRP7Tormimrpt Merged SuperSetRefammce RR4937 <br />