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' COLUMBIA ANALYTICAL SERVICES,INC <br /> Analytical Results <br /> Client Applied Earth Sciences, Incorporated Service Request X0400795 <br /> I Protect Canteen Corp/AGE-NC-99-0512 Date Collected 08/16/2004 <br /> mple Matrix Water Date Received 08/17/2004 <br /> Volatile Organic Compounds <br /> Sample Name MW-3D/081604 Units ug/L <br /> Lab Code X0400795-003 Basis NA <br /> Extraction Method EPA 5030B Level Low <br /> Analysis Method 8260B <br /> Dilution Date Date Extraction <br /> Analyte Name _ _ Result Q,., MRL MDL Factor Extracted Analyzed Lot Note <br /> Methyl tert-Butyl Ether 75 10 080 1 08/30/04 08/30/04 XWG0400953 <br /> Benzene 23 050 030 1 08/30/04 08/30/04 XWG0400953 <br /> 1,2-Dichloroethane ND U 050 050 1 08/30/04 08/30/04 XWG0400953 <br /> Toluene ND U 0 50 020 1 08/30/04 08/30/04 XWG0400953 <br /> 1,2-Dibromoethane ND U 0 50 030 1 08/30/04 08/30/04 XWG0400953 <br /> Ethylbenzene 2 6 050 020 1 08/30/04 08/30/04 XWG0400953 <br /> 1 m,p-Xylenes ND U 10 060 1 08/30/04 08/30/04 XWG0 000953 <br /> o-Xylene ND U 0 50 030 1 08/30/04 08/30/04 XWG0400953 <br /> tent-Butyl Alcohol ND U 20 10 1 08/30/04 08/30/04 XWG0400953 <br /> Dnsopropyl Ether ND U 10 040 1 08/30/04 08/30/04 XWG0400953 <br /> tert-Amyl Methyl Ether ND U 050 030 1 08/30/04 08/30/04 XWG0400953 <br /> tent-Butyl Ethyl Ether ND U 050 030 1 08/30/04 08/30/04 XWG0400953 <br /> 1 • <br /> 1 Control Date <br /> Surrogate Name %Rec Limits Analyzed Note <br /> Dibromofluoromethane 92 77-121 08/30/04 Acceptable <br /> 1 Toluene-d8 90 65-131 08/30/04 Acceptable <br /> 4-Bromofluorobenzene 75 68-125 08/30/04 Acceptable <br /> 1 <br /> 1 <br /> I <br /> 1 I <br /> I <br /> ants <br /> Printed 09/20/2004 11 51 12 Form IA-Organic Page 1 of I <br /> L\STEALTMCRYSTAL RPT1Fomstm rpt Mcrged SuperSet Rcfcrcnce RR4937 <br />