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May-28-03 04 05Rm From-Gettler-Ryan Inc +925 551 7889 7-751 P 020/025 F-960 <br /> IfLancaster <br /> Laboratories Analysis Report <br /> 2425 Naw Hafand Pike,PO Box 12425 tancsster,PA 178052425-717858.2300 Faz 717.6562681-www lancasterlabs corn <br /> Page Y of 5 <br /> Quality Control Sux=ary <br /> Client Name- Ch,eVronTexaco Group Number 850557 <br /> Reported 05/16/03 at 05 09 PM <br /> Laboratory Compliance Quality Control <br /> ]Blank Blank Report x.CS LcSD LCS/LCSD <br /> An Name U13,311t IIzfl[A RE $R8C Limzt@ RPD Maur <br /> Batch number 0312SO014A Sample number{,) 4037607-4037614 <br /> TPH - DRO CA LUPT (Watex6) N n SD ug/1 301 140 61-126 1 20 <br /> Batch number 031250020A Sample nu+riber(s) - 4037611-4037614 <br /> Methanol (by Direct In]ectaon) N D 200 ug/l 109 78-114 <br /> Batch number 03125112603.A Sample number s) 4037615 <br /> TRPH 418 1 N D 0 25 mg/1 92 54-113 <br /> Batch number 03126AD7C sample number(s) 4037606-4037609 <br /> TPN-GRO - water8 N D 50 ug/3- 89 92 70-130 3 30 <br /> Batch number 03127A07B Sample number(s) 4037610-4037615 <br /> TPH-GRC - waters N D 50- ug/1 99 70-130 <br /> Batch number N031272AH Sample number(a) 4037511-4037615 <br /> Ethanol N D 50 ug/1 99 43-159 <br /> Methyl Tertiary Butyl Ether N D o 5 ug/1 103 77-127 <br /> dx-Isopropyl ether N D D 5 u9/1 98 74-125 <br /> Ethyl t-butyl. ether N D 0 5 ug/1 96 74.120 <br /> t-Amyl methyl ether N D 0 5 ug/l 95 79-113 <br /> e-Butyl alcohol N D 5 ug/l 106 53-147 <br /> Benzene N A 0 5 ug/1 108 8S-117 <br /> 0 2-D1chloromthane N D 0 5 ug/1 101 77-132 <br /> oluene N D 0 5 ng/1 102 85-115 <br /> 2-t)abromoethane N D 0 5 u9/1 104 H1-114 <br /> Ethylbentenc N D p 5 u5/1 99 82-119 <br /> Xylene (Total) N D 0 5 ug/1 105 84-120 <br /> Batch number N031201AB Sample number s) 4037610 <br /> Methyl Tertiary Butyl Ether N D O 5 ug/l 107 77-127 <br /> Hen2ene N D 0 5 ug/1 109 ES-117 <br /> Toluene N D D 5 u9/1 102 85-115 <br /> Ethylbenzene N D 0 5 ug/1 1DO 82_119 <br /> Xylene (Total) N D 0 5 ug/1 106 84-120 <br /> Batch number P031331AA Sample number(s) 4037607 <br /> Methyl Tertiary Butyl Ether N D 0 5 ug/1 99 77-127 <br /> Benzene N D 0 5 ug/l 104 H5-117 <br /> Toluene N D 0 5 ug/l 99 A5-115 <br /> Ethylbenzene N D 0 S ug/1 100 82-119 <br /> xylene (Total) N D 0 5 ug/1 101 84-120 <br /> Batch number P031332AA Sample number(c) 4037608 <br /> Methyl Tertiary Butyl Ether N D 0 S 13g/1 97 77-127 <br /> Benzene N D 0 S <br /> ug/1 304 85-117 <br /> Toluene N D 0 5 ug/1 101 85-115 <br /> Ethylbenzene N D D 5 ug/1 101 82-119 <br /> xylem {Total) N D 0 5 ug/l 100 <br /> 84-124 <br /> Batch number P031-132AD Sample number(e) 4037606,4037609 <br /> Merhyl Tertiary Butyl Ether N D 0 Sug/1 97 77-137 <br /> Benzene N n 0 S ug/>, 10D 85-117 <br /> Toluene N 2] 0 5 u9/1 101 65-115 <br /> Ethylbenzene N D D 5 ug/1 201 82-119 <br /> Outside of specification <br /> (]) The result fer one or both dcterm)nations was less than five times the LOQ <br /> (2) The background result was more than four tames the spike added <br />