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May-28-03 04 05pm From-Gettler-Ryan Inc +925 551 7899 T-751 P 021/025 F-964 <br /> Lancaster <br /> Laboratories A n a I ysis Report <br /> 2425 New Hollam Pike,PO Bar 12425,Lancaster,PA 176052425-717-656-2:300 Fax 717-GS&RO81-www-larleastarlabsCOM <br /> Page 2 of S <br /> Quality Control Summary <br /> Client Name ChevxonTexaco Group Number 650557 <br /> Reported 05/16/03 at 05-09 PM <br /> Laboratory -'Compliance Quality Control <br /> 81ank Black Report LCS Lesn LCS/LCSD <br /> Ann IYaae_Name Rcaulc M& M9jL to %BE NO—C! its RPR REP-Mai[ <br /> Xylene (Total) N-D 0 5 uy/1 lQ0 64-12U <br /> Sample Matrix Quality Control <br /> MS XSD r1S/XSD kPn 8KG DUP Dur nup� <br /> Anal ame 4 EC !EEC ,T,imiCa RPDRRy'D <br /> X cong cone RPL <br /> Batch number 031250020A Sample nvmber(a) 4037611-4037614 <br /> methanol (by Direot Ynaecrxon) 104 113 78-116 a 20 <br /> Batch number 0-1125142601A Sample riumber(s) 4037615 <br /> TRPH 418 1 77 86 39-132 10 14 1 5 9 5 145" (1) 34 <br /> Stitch number 03126A07C Sample numbers) 4037606-4037609 <br /> TPH-GRO - Water's 116 70-130 <br /> Bacch number 03127A07B Sample number(93) 4037610-4037615 <br /> TPH-GRO - Water& 115 115 70-130 0 130 <br /> Batch number N031272AB Sample number(e) 4037611-4037615 <br /> Ethanol 99 112 34-163 13 30 <br /> •Methyl Tertiary Butyl, Ether 105 106 69-134 0 30 <br /> di-isopropyl ether 103 102 75-130 1 30 <br /> Ethyl t-butyl ether 100 99 73-123 2 30 <br /> r-Amyl methyl ether 98 99 77-117 2 30 <br /> t-Butyl alcohol 114 118 39-155 3 30 <br /> Benzene (2) (2) 93-128 1 30 <br /> 1 2-Dichloroethane 130 127 73-136 2 30 <br /> Toluene 111 109 83-127 1 30 <br /> 1,2-Dibroigoethane 107 106 78-120 1 30 <br /> Ezhylbenzene 150- 127 82-134 9 30 <br /> Xylene (Total) 129 116 82-130 6 30 <br /> batch number MD31281AB sample number(a) 4037610 <br /> Methyl Tertiary Butyl Ether 108 108 59-134 0 30 <br /> Benzene 118 119 83-128 1 30 <br /> Toluene 111 112 83-127 1 30 <br /> Ethylbenxenc 107 108 82-13e 1 30 <br /> xylene (Total) 112 114 82-130 1 30 <br /> Batch number P031331AA Sample number(0) 4037607 <br /> Methyl Tertiary Butyl Ether 100 99 69-134 4 30 <br /> BCnzene 109 107 83-128 1 30 <br /> Toluene 102 106 63-127 3 30 <br /> EthylbCnlene 103 104 82-134 0 30 <br /> Xylene (Total) 104 105 82-130 1 30 <br /> Batch number P031332AA Sample number(~) 40375oB <br /> Methyl Tertiary Butyl Echer 97 101 69-134 4 3D <br /> Benzene 105 Ill 83-128 5 30 <br /> TD-�uCne 103 109 83-127 6 30 <br /> Ethylbenzehe 104 111 82-134 6 30 <br /> lylene (Total) 103 109 62-130 6 34 <br /> *-Outside of specification <br /> (1) The result for one or both determinations was less than five tuneS rhe LOQ <br /> (2) The background res-ult was more than four times the spike added <br />