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Curtis & Tompkins Labs GC/MS CONTINUING CALIBRATION REPORT FOR MSVOA04 ma File: def12 Date Analyzed: 15-MAY-2000 Time Analyzed: 14 :43 t Cal Date: 14-MAY-00 Meth: \\gcrosserver\dd\chem\msvoa04 . i\051500 .b\i4m826w.m Compound RF RF MinRF Actual Ouant WD Max Flags Hexane COMPOUND NOT DEFECTED 1-Chlorohexane COMPOUND NOT DETECTED 1,4-Dioxane COMPOUND NOT DETECTED Freon 12 0.3971 0.3949 0 0500 50 00 49.73 -1 30 Chloromethane 0.2976 0.2899 0 1000 50.00 48.70 -3 30 Vinyl Chloride 0.2641 0.2838 0 0500 50.00 53.72 7 20 Bromomethane 0.2441 0.2025 0.0500 50.00 46.10 -8 30 Chloroethane 0.1612 0.1549 0 0500 50.00 48 05 -4 30 Ethanol 0.0016 0.0009 0.0005 5000.00 2664.34 -47 4 1y Trichlorofluoromethane 0.4301 0.4566 0 0500 50.00 53.08 6 30 Isopropanol 0.0109 0.0065 0 0050 500.00 297.71 -40 40 Acetone 0.0887 0.0788 0 0500 50.00 44 42 -11 40 Freon 113 0.2688 0.3105 0 0500 50 00 49 56 -1 30 l,l-Dichloroethene 0.2506 0.2362 0 0500 50.00 47.13 -6 20 Methylene Chloride 0.3980 0.3783 0.0500 50.00 47.53 -5 30 Carbon Disulfide 1.0487 1.0077 0 0500 50.00 48.04 -4 30 MTBE 1.1908 1.0435 0 0500 50.00 43 82 -12 30 trans-1,2-Dichloroethene 0 3665 0.3390 0.0500 50 00 46 26 -7 30 Vinyl Acetate 0 7630 0.6416 0.0500 50 00 42 04 -16 40 1,1-Dmchloroethane 0 6731 0.6159 0.1000 50 00 45.75 -8 30 • 2-Butanone 0 1732 0.1441 0 0500 50.00 41.61 -17 40 2,2-Dichloropropane 0 5400 0 4310 0 0500 50 00 44 83 -10 30 cis-1,2-Dichloroethene 0 4229 0 3826 0 0500 50.00 45 24 -10 30 Chloroform 0 7079 0 6429 0 0500 50.00 45.41 -9 20 Bromochloromethane 0 2135 0 1928 0.0500 50.00 45 15 -10 30 Dibromofluoromethane 0 4725 0 4734 0.0500 50.00 50.10 0 30 Tetrahydrofuran 0.1029 0 0872 0 0050 500.00 423 77 -15 40 1,1,1-Trichloroethane 0 4983 0 4934 0 0500 50.00 49.51 -1 30 1,1-Dichloropropene 0 3432 0.3334 0 0500 50.00 48.58 -3 30 1,2-Dichloroethane-d4 0 3774 0.3738 0 0500 50 00 49.53 -1 30 Carbon Tetrachloride 0 3144 0.3228 0.0500 50 00 51.33 3 30 1,2-Dichloroethane 0 3908 0 3504 0 0500 50.00 44 82 -10 30 Benzene 1 1673 1.0687 0 0500 50.00 45.77 -8 30 , Trichloroethene 0 2852 0.2722 0 0500 50.00 47.72 -5 30 1,2-Dichloropropane 0 3068 0.2812 0 0500 50.00 45.84 -8 20 Bromodichloromethane 0.4053 0 3745 0 0500 50.00 46 20 -8 30 D3.bromomethane 0.1877 0.2002 0.0500 50.00 48 21 -4 30 2-Chloroethylvinyiether 0 1290 0.1150 0 0500 50.00 44 58 -11 40 4-Methyl-2-Pentanone 0.2516 0.2195 0 0500 50.00 43.62 -13 40 cis-1,3-Dichloropropene 0 4774 0.4215 0.0500 50.00 44.14 -12 30 Toluene-d8 1.1173 1.1099 0.0500 50 00 49.67 -1 30 Toluene 0.6828 0.6158 0 0500 50 00 45 09 -10 20 trans-1,3-Dichloropropene 0.4134 0.3795 0 0500 50 00 45.90 -8 30 1,1,2-Trichloroethane 0 1595 0.1465 0 0500 50 00 45 93 -8 30 2-Hexanone 0 1919 0.1694 0.0500 50.00 44.14 -12 40 agFAIL y=in CCS P Pagee 1 of 2