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Curtis & Tompkins Labs GC/MS CONTINu:m CALIBRATION REPORT FOR MSVOA04 Data File: def12 Date Analyzed: 15-MAY-2000 Time Analyzed: 14:43 Init Cal Date: 14-MAY-00 Meth: \\gcrosserver\dd\chem\msvoa04 . i\051500 .b\i4m826w.m C Hund RF RF MinRF Actual QMant VD Max Flacro 1,3-D3.chloropropane 0.5210 0 4776 0.0500 50.00 45.83 -8 30 Tetrachloroethene 0.3251 0.3330 0.0500 50.00 51.21 2 30 Dibromochloromethane 0.3579 0.3419 0.0500 50.00 47.77 -4 30 1,2-Dibromoethane 0 2508 0.2364 0.0500 50.00 47.14 -6 30 Chlorobenzene 0.8551 0 7996 0.3000 50.00 46.75 -6 30 1,1,1,2-Tetrachloroethane 0.3241 0.2994 0.0500 50.00 46.18 -8 30 Sthylbenzene 1.5119 1.4008 0.0500 50.00 46.33 -7 20 m,p-Xylenes 0 5403 0.5050 0.0500 100.00 93 47 -7 30 o-Xylene 0.5362 0.4999 0.0500 50.00 46.62 -7 30 Styrene 0.9263 0.8700 0.0500 50.00 46.96 -6 30 Bromoform 0.2367 0.2285 0.1000 50.00 48.27 -3 30 Cyclohexanone 0 0128 0.0054 0 0050 500.00 211..25 -58 40 Isopropylbenzene 2 2449 2 1346 0.0500 50.00 47 54 -5 30 N 1,1,2,2-Tetrachloroethane 0 6526 0.5592 0.3000 50.00 42 84 -14 30 Bromofluorobenzene 0.8977 0.8892 0 0500 50.00 49.53 -1 30 1,2,3-Trichloropropane 0.1645 0.1.268 0.0500 50.00 44 74 -11 30 Propylbenzene 2.8306 2.6977 0.0500 50 00 47.65 -5 30 • Bromobenzene 0 6985 0 6408 0.0500 50.00 45.87 -8 30 2-Chlorotoluene 1 9281 1.7510 0.0500 50 00 45 41 -9 30 1,3,5-Trimethylbenzene 1.7044 1 6207 0.0500 50.00 47.55 -5 30 4-Chlorotoluene 1 8331 1 7055 0.0500 50 00 46 52 -7 30 tert-Butylbenzene 1 6189 1 5150 0.0500 50.00 46.53 -7 30 1,2,4-Trimethylbenzene 1 6202 1.5378 0.0500 50.00 47.46 -5 30 sec-Butylbenzene 2 2400 2 1492 0.0500 50 00 47.97 -4 30 para-Isopropyl Toluene 1 7910 1 7331 0.0500 50.00 48.38 -3 30 1,3-Dichlorobenzene 1 2399 1 1533 0.0500 50.00 46.51 -7 30 1,4-Dichlorobenzene 1 2685 1.1691 0 0500 50.00 46 08 -8 30 n-Butylbenzene 1 5045 1 5004 0 0500 50 00 49 86 0 30 1,2-Dichlorobenzene 1 1678 1 0928 0.0500 50.00 46.79 -6 30 1,2-Dibroma-3-Chloropropane 0.1057 0 0889 0.0500 50.00 43 17 -14 30 1,2,4-Trichlorobenzene 0 4070 0 4394 0.0500 50 00 44.94 -10 30 Hexachlorobutadiene 0 3383 0.3164 0.0500 50.00 46 76 -6 30 Naphthalene 0 5792 0.4615 0.0500 50.00 37 19 -26 30 1,2,3-Trichlorobenzene 0 3733 0 3953 0.0500 50 00 43.63 -13 30 Internal Standard Co=ound ICS Area CCS ,Area Diff W ICS RT CCS RT Diff Pentafluorobenzene 630626 631371 +0 12 9 44 9 .44 0 00 1,4-Difluorobenzene 831705 825597 -0.73 10.95 10.94 0 00 Chlorobenzene-d5 700455 689644 -1.54 16.01 16 01 0 00 1,4-Dichlorobenzene-d4 420554 408896 -2 .77 20.33 20.33 0.00 i 154 1=CAL FAIL y=in CCS