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110 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAUTBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> Ihap JLwww Mrgamphell corn E-mail mam@mccampbeIl com <br /> Advanced GeoEnvironmental Client Project ID Chase-Van Buren Date Sampled 11/04/98 <br /> 4005 North Wilson Way <br /> Date Received 11/06/98 <br />' Stockton, CA 95205 Client Contact Kevin McKibben Date Extracted 11/08/98 <br /> Client P O Date Analyzed 11/08/98 <br />' Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 98253 <br />' Client ID MW-3/11-4-98 <br /> Matnx W <br /> Compound Concentration* Compound Concentration* <br /> I Acetone ND<4400 Ethylbenzene 4400 <br /> Benzene 15,000 Hexachlorobutadiene ND<1300 <br /> Bromobenzene ND<1300 Iodomethane ND<1300 <br /> Bromochioromethane ND<1300 lsopropylbenzene ND<1300 <br /> Bromodichloromethane ND<1300 p-Isopropyl toluene ND<1300 <br /> Bromoform ND<1300 Methyl butyl ketone NIX1300 <br /> Bromomethane ND<1300 Methylene Chloride"' ND<1300 <br /> n-Butyl benzene NIX1300 Methyl ethyl ketone ND<1300 <br />' sec-Butyl benzene ND<1300 Methyl isobutyi ketones ND<1300 <br /> tert-Butyl benzene ND<1300 Methyl tert-Butyl Ether(MTBE) <br /> Carbon Disulfide ND<1300 Napthalene ND<1300 <br /> I • Carbon Tetrachlonde ND<1300 n-Propyl benzene ND<1300 <br /> Chlorobenzene ND<1300 Styrene M ND<1300 <br /> Chloroethane ND<1300 1,1,1,2-Tetrachloroethane ND<1300 <br /> 2-Chloroethyl Vinyl Ether" ND<1300 1,1,2,2-Tetrachloroethane ND<1300 <br /> Chloroform N13<1300 Tetrachloroethene ND<1300 <br /> Chloromethane NIX1300 Toluene 60,000 <br /> 2-Chlorotoluene ND<1300 1,2,3-Tnchlorobenzene N EX 1300 <br /> 4-Chlorotolucne ND<1300 1,2,4-Tnchlorobenzene ND<1300 <br /> Dibromochloromethane NIX1300 1,1,1-Tnchioroethane ND<1300 <br /> 1,2-Dibromo-3-chloropropane ND<1300 1,1,2-Tnebloroethane ND<1300 <br /> Dibromomethane ND<1300 Trichloroethene ND<1300 <br /> 1,2-Dichlorobenzene ND<1300 Tnchlorofluoromethane ND<1300 <br /> 1,3-Dichlorobenzcne ND<1300 1,2,3-Tnchl oropropane ND<1300 <br /> 1,4-Dichlorobenzene ND<1300 1,2,4-Tnmethylbenzene 2700 <br /> Dichlorodifluoromethane ND<1300 1,3,5-Tnmethylbenzene ND<1300 <br /> 1,1-Dichloroethane ND<1300 Vinyl Acetate ° NIX1300 <br /> 1,2-Dichloroethane NIX1300 Vinyl Chloride t° ND<1300 <br /> l,l-Diebloroethene ND<1300 Xylenes,total 26,000 <br /> cis-1,2-Dichloroethene ND<1300 <br /> trans-l,2-Dichlomethene ND<1300 <br /> ],2-Dichloropropane ND<130f1 <br /> 1,3-Dichloropropane ND<1300 <br /> 2,2-Dichloropropane ND<1300 Comments <br /> 1,1-Dichloropropene ND<1300 Surrogate Recoveries(%) <br /> cis-1,3-Dichloropropene ND<1300 Dibromofluoromethane 95 <br /> trans-1,3-Dichloropropene ND<1300 Toluene-d8 103 <br /> Ethylene dibromide NI3<1300 4-Bromofluorobenzene 102 <br /> I water and vapor samples are reported m uglL,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts m ug/L <br /> Reporting limas unless otherwise stated water samples 10 ug/L, vapor samples 0 5 ug/L, solid and sludge samples 5 ug/kg, wipes <br /> 0 2ug/wipe ND means not detected above the reporting limit,N/A means analyte not applicable to this analysts <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pemanone or isopropylacetone,(h) lighter than water immiscible sheen is present, (i)liquid sample that contains greater than --5 vol % <br /> sediment,0)sample diluted due to high organic content, (k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte,Q)methylbenzene,(m)acetic acid ethenyl ester,{n)chloroeihene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />